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《Journal of Anhui University(Natural Science Edition)》 2012-03
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Synthesis and characterization of N,N-dibutyl dithiocarbamate antimony

LI Lai-xing1,2,WU Bing3,ZHANG Yu-chuan1,2(1.College of Chemistry and Chemical Engineering,Anhui University,Hefei 230039,China; 2.Anhui Province High Performance Rubber Materials and Products Laboratory,Hefei 230088,China; 3.Anhui Anda Zhongding Rubber Technology Development Co.,Ltd,Hefei 230088,China)  
A complex N,N-dibutyl dithiocarbamate antimony(SDBC) was synthesized by one-step method.The results of IR,13C-NMR,EA and ICP test indicated that the composition and structure of the product accord with the target product and the coordination number of SDBC is 3.Moreover,the DSC curve showed a single and narrow peak at 73 ℃,which indicates that the melting point of the product is 73 ℃ and the purity of the product is extremely high.Finally,the TGA curve showed that there is an obvious weight loss when the temperature is above 220 ℃,SDBC exhibits a good thermal stability.
【CateGory Index】: O627.5
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