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Studies on the Polysaccharides from Changium smyrnioides Wolff

Zhang Linwei Wu Dongru Zhao Zhiping Zhou Enzhi (Biology Department.Anhui University Hefei 230039)  
Two polysaccharides ,CSP 1 and CSP 2,were obtained from Changium smyrnioides Wolff. They were proved to be homogenous by electrophoresis and gel filtration.Two ratio 1:4.M.W. of CSP 1 and CSP 2 were 500KD and 18KD respectively.CSP 1 and CSP 2 showed positive specific rotation: 18 D =+218(c=0.1,H 2O)for CSP 1, 18 D =+10,33(c=0.1,H 2O)for CSP 2.CSP 1 contained galatose and xylose,CSP 2 contained glucose,rahmnose and fructose.CSP 2 also contained uronuc acid indicated by Discher method.I.R.spectra and H NMR suggested that both CSP 1 and CSP 2 have α-glycoside linkage.From the results of pemodate oxidation and Smith detration,it was estimated that CSP 1 only had 14 linkage and that CSP 2 had 16 and 13 linkages.
【CateGory Index】: Q949.59
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