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《Anhui Chemical Industry》 2009-04
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Improved Synthesis of Trichlorosucrose

NIU Tao,ZHU Ren-fa,SHAO Guo-quan (Department ofChemical and Materials EngineeringofHefei University,Hefei 230022,China)  
Sugar was as the start material by the reaction of ester exchange,chlorination (Vilsmeier),deacetyl in three steps obtained the trichlorosucrose. The improvement of the synthesis procedure is simplicity and convenient. The reaction condition is moderate and the starting material is very cheap to get. The total yield is increased to 39.4% from 35% yield of the reference.
【CateGory Index】: TS264.9
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【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 ZHU Ren-fa1,SHAO Guo-quan1,HE Yong2(1.Department of Chemistry and Material Engineering,Hefei University,Hefei 230022,China;2.Hefei Huijia Chemical Industry Sci & Tec Co LTD,Hefei 230051,China);Improved synthesis of a novel high intensity sweetener trichlorosucrose[J];Journal of Anhui University(Natural Sciences);2008-01
2 Zhou Weiyi Deng Xiaojuan Kuang Qing(Analysis Center,Tianjin University,Tianjin,300072);Gas chromatographic determination of dimethyl formamide for recovery.[J];Analytical Instrumentation;2008-01
3 Ni Jun-ming1, LI Jun-ping2 (1.Guangzhou Hua Qiao Sugar company, Guangzhou 510165, China) (2.South China University of Technology, Food science& Bioengineering college Guangzhou, 510640,China);Research and Developing Prospects on Processing Techniques of Saccharose[J];Guangzhou Food Science and Technology;2005-02
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5 LIU Kui~1,RONG Xin-yu~2 (1. College of Sciences, Hebei University of Science and Technology,Shijiazhuang Hebei 050018,China;2. College of Chemical and Pharmaceutical Engineering, Hebei University of Science and Technology. Shijiazhuang Hebei 050018,China);Research Progress and Development Prospect of High-intensive Sweetener — Sucralose[J];Hebei Journal of Industrial Science & Technaology;2004-04
6 WU Xiao-yu,ZHANG Wei-xing,WU Wei-hong,HUANG Lin-jun(College of Material Science and Chemical Engineering,Zhejiang University,Hangzhou 310027,China);Preparation of Trispa——the Intermediate of Trichlorosucrose[J];Chemistry & Bioengineering;2006-07
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Chinese Journal Full-text Database 4 Hits
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