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《Anhui Chemical Industry》 2009-04
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Improved Synthesis of Trichlorosucrose

NIU Tao,ZHU Ren-fa,SHAO Guo-quan (Department ofChemical and Materials EngineeringofHefei University,Hefei 230022,China)  
Sugar was as the start material by the reaction of ester exchange,chlorination (Vilsmeier),deacetyl in three steps obtained the trichlorosucrose. The improvement of the synthesis procedure is simplicity and convenient. The reaction condition is moderate and the starting material is very cheap to get. The total yield is increased to 39.4% from 35% yield of the reference.
【CateGory Index】: TS264.9
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Chinese Journal Full-text Database 10 Hits
1 ZHU Ren-fa1,SHAO Guo-quan1,HE Yong2(1.Department of Chemistry and Material Engineering,Hefei University,Hefei 230022,China;2.Hefei Huijia Chemical Industry Sci & Tec Co LTD,Hefei 230051,China);Improved synthesis of a novel high intensity sweetener trichlorosucrose[J];Journal of Anhui University(Natural Sciences);2008-01
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