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《Journal of Anhui Agricultural Sciences》 2006-10
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Simultaneously Determination of Four Effective Components in Swertia tetraptera Maxim.by HPLC

LIANG Yong-xin et al(Chemistry Department of Qinghai Nationalities Institutes,Xining,Qinghai 810007)  
To establish a quantitative method of simultaneously determination of loganic acid,swertiamarin,gentiopicroside and mangiferin in Swertia tetraptera Maxim.by RP-HPLC.Method: The sample were separated on the column of Zorbax SB-C18(250 mm×4.6 mm i.d.,5 μm)which eluted with methanol and water(0.04 % phosphoric acid).The ratio of methanol and water increased from 20∶80 to 35∶65 in 20 min with detected wavelength at 254 nm,flow rate at 1 ml/min,column temperature at 30 ℃.Results: Four compounds were base-isolated.The linear ranges of loganic acid,swertiamarin,gentiopicroside and mangiferin were 0.05~0.625 μg(r=0.999 9),0.095~2.9 μg(r=0.999 8),0.049~2.56 μg(r=0.9997),0.006~2.8 μg(r=0.999 9)respectively,the average recoveries were 101 %(RSD=4.3 %),98.7 %(RSD=3.3 %),99.5 %(RSD=3.5 %),102 %(RSD=1.0 %)respectively.Conclusions: the method is rapid and precise.
【CateGory Index】: R284
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