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《Journal of Anhui Agricultural Sciences》 2007-29
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Study on the Determination Method of the Residual Quantity of Multi-Organophosphorus Pesticides in Honey

SUI Wu-Bin(Department of Chemistry,Zaozhuang College,Zaozhuang,Shandong 277101)  
[Objective] The purpose was to seek for the optimum method to detect the residual quantities of multi-organophosphorous pesticides in honey.[Method] With DB-35 silica capillary column for split stream sampling and programmed heating,flame photometric detector(FPD) with optical filter with phosphorous for detecting,and high purity nitrogen,air and hydrogen as carrier gas,the method of detecting the residual quantities of 8 organophosphorous pesticides(DDVP,methamidophos,phorate,dimethoate,methyl parathion,malathion,chlorpyrifos and parathion) in honey by gas chromatography method was established.[Result] 8 kinds of organophosphorous pesticides had good linear relationship(r0.995 5) in the content range of 1~100 ng/mL,their least detective ranges were 0.021~0.1 μg/mL and the additive recoveries were in 81 %~100 %.[Conclusion] The accuracy,sensitivity,recovery and reproducibility of the method all accorded with the requirement of detective technique of pesticide multi-residue.
【CateGory Index】: S896.1
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【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 ZHAO Er-Cheng et al(Chinese Agricultural University,Beijing 100094);Research Advance in the Residue Analysis of Plant Growth Regulator[J];Journal of Anhui Agricultural Sciences;2005-09
2 SUI Wu-bin(Department of Chemistry,Zaozhuang University,Zaozhuang,Shandong 277101);Study on Organophosphorus Pesticide Residue in Chinese Medicinal Material[J];Journal of Anhui Agricultural Sciences;2008-05
3 Li Shuang1,Du Wei2,Li Shoufu1(1.Heilongjiang Environmental Protection Research Institute,Harbin 150056,China; 2.Dongning Environmental Monitoring Station,Dongning 157200,China);Determination of Trichlorfon Residues in Water by Pyrolysis Gas Chromatography[J];Environmental Science and Management;2009-07
4 HUANG Hong-lin, LIU Shi, ZHANG Tao-zhi~* (Center of Testing and Analysis, Central China Normal University, Wuhan 430079);Determination of Gibberellin Residue in Tomato by Solid Phase Extraction-High Performance Liquid Chromatography[J];Journal of Analytical Science;2005-01
5 LIU Yong*,YANG Chang-zhi and KANG Qing-he(Technology Center of Heilongjiang Entry-Exit Inspection and Quarantine Bureau,Harbin 150001);Determination of trichlorfon residues in foodstuffs of animal origin by pyrolysis gas chromatography[J];Chinese Journal of Analysis Laboratory;2008-02
6 JIANG Ting,ZHANG Guo-wen* and WANG An-ping(Key Laboratory of Food Science of Ministry of Education,Nanchang University,Nanchang 330047);Study on interaction of bromocresol green-triton X-100 with prometryne by resonance light scattering measurements[J];Chinese Journal of Analysis Laboratory;2008-06
7 PENG Jing-He HUANG Gao-Ling ZHANG Yong ZHU Ya-Xian a (Key Laboratory of Marine Environmental Science of MOE,Xiamen University,Xiamen,Fujian 361005,P.R.China) a(Department of Chemistry,Xiamen University,Xiamen,Fujian 361005,P.R.China);Room Temperature Phosphorescence of Carbaryl Induced by β-Cyclodextrin in the Presence of Heavy Atom Perturbation[J];Chinese Journal of Spectroscopy Laboratory;2004-04
8 SONG Zheng-ping,TIAN Shi-long,WANG Dong-hui,ZHU You-chun(Testing Center,Gansu Academy of Agricultural Sciences,Lanzhou 730070,China);An Analytical Study on Organophosphorus and Carbamate Pesticide Residues in Vegetables by GC-TSD[J];Journal of Gansu Sciences;2006-02
9 ZHANG Yan(The Supervision and Testing Center for Lycium Quality,Ministry of Agriculture,Yinchuan Ningxia 750002,China);Evaluation Different Extraction Solvent in Analysis of Pesticide Residues[J];Gansu Agricultural Science and Technology;2006-09
10 HAN Yan1,2 (1.State Key Laboratory of Marine Environmental Science,Environmental Science Reasearch Center, Xiamen University,Xiamen Fujian 361005,China; 2.School of Chemistry and Chemical Engineering,Fuyang Teachers College,Fuyang Anhui 236032,China);Simultaneously determination of some organophosphorus pesticide residues in vegetables[J];Journal of Fuyang Teachers College(Natural Science);2009-02
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