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《Journal of Anhui Agricultural Sciences》 2008-02
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Study on Simultaneous Detection of 3 Tetracyclines Residues in Eggs by High Performance Liquid Chromatography

ZHANG Yin-zhi et al (The State Key Lab of Food Science and Technology, Wuxi, Jiangsu 214122)  
A new method for the determination of 3 tetracyclines ( TCs) by high performance liquid chromatography (HPLC) was proposed in eggs. TCs were separated on a Diamonsil C18 column(250 mm ×4.6 mm i.d., 5 μm) using methanol-acetonitrile-0.01 mol/ L oxalic acid(pH 2.5)with a flow rate of 1.0 ml/min and detecting at 358 nm. The result showed that the limits of detection were 0.25, 0.11, 0.52 μg/ml for oxytetracycline(OTC), chlortetracycline (CTC), tetracycline (TC), resp. and the standard curve was at good linear. The relative standard deviation (RSD) of OTC, CTC and TC were 1.94 %, 1.20 %, 0.84 %, resp. The effects of the distribution proportion of the mobile phase, pH value and the acetic acid concentration on separation were discussed.
【Fund】: 江苏省质监局立项项目(20062B24);; 江南大学211师资基金项目
【CateGory Index】: S859.84
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