Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Journal of Anhui Agricultural Sciences》 2008-02
Add to Favorite Get Latest Update

Study on Simultaneous Detection of 3 Tetracyclines Residues in Eggs by High Performance Liquid Chromatography

ZHANG Yin-zhi et al (The State Key Lab of Food Science and Technology, Wuxi, Jiangsu 214122)  
A new method for the determination of 3 tetracyclines ( TCs) by high performance liquid chromatography (HPLC) was proposed in eggs. TCs were separated on a Diamonsil C18 column(250 mm ×4.6 mm i.d., 5 μm) using methanol-acetonitrile-0.01 mol/ L oxalic acid(pH 2.5)with a flow rate of 1.0 ml/min and detecting at 358 nm. The result showed that the limits of detection were 0.25, 0.11, 0.52 μg/ml for oxytetracycline(OTC), chlortetracycline (CTC), tetracycline (TC), resp. and the standard curve was at good linear. The relative standard deviation (RSD) of OTC, CTC and TC were 1.94 %, 1.20 %, 0.84 %, resp. The effects of the distribution proportion of the mobile phase, pH value and the acetic acid concentration on separation were discussed.
【Fund】: 江苏省质监局立项项目(20062B24);; 江南大学211师资基金项目
【CateGory Index】: S859.84
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
Chinese Journal Full-text Database 3 Hits
1 ZHANG Yin-zhi et al(National Key Lab of Food Science and Technology,Southern Yangtze University,Wuxi,Jiangsu 214036);Study of Rapid Detection on Tetracycline Antibiotics in Food by Using Gold-labeled Reagent Strip[J];Journal of Anhui Agricultural Sciences;2008-27
2 WANG Hong-bo,GAO Ya-qin,DU Tian-qing,NIU Chun-e,LI Wei-hong(Quality Supervising,Inspecting and Testing Center for Animal Fiber,Fur,Leather and Products(Lanzhou),MOA,P.R.China;Lanzhou Institute of Animal Science and Veterinary Pharmaceutics,CAAS,Gansu,Lanzhou 730050,China);The Hazards of Antibiotic Residues in Milk and Detection Method Overview[J];Animal Husbandry and Feed Science;2010-04
3 WANG Fei,LIU Wen-ying,ZHAO Wei-gao,HUANG Li-yan,ZHANG Qiang, WANG Xu-qing,HAN Zhao-peng, LU Xiao-ming(Chinese National Egg Engineering Research Center,Beijing 102115,China; Beijing DQY Agriculture Technology Co.Ltd,Beijing 100081,China);Research Progress on Safety Detection of Eggs[J];Academic Periodical of Farm Products Processing;2012-08
China Proceedings of conference Full-text Database 2 Hits
1 FANG Zhong-yi LIU Sui-mei SONG Zhi-chao (Henan provincial supervising agency of veterinary Drugs,Zhengzhou,450008;China);Determination of 4 Tetracyclines in Eggs by High Performance Liquid Chromatography[A];[C];2008
2 LU Guang-ju ZHAOYing SUN Zhi-wen WANGYing (Beijing Institute of Veterinary Drug Control,Beijing 100107;China);Determination of Oxytetracyline,Tetracycline and Chlortetracycline Residues in Egg and Beef by UPLC[A];[C];2008
Chinese Journal Full-text Database 3 Hits
1 WANG Lei, ZHANG Xiao song, XU Zhi xiu, SHAO Xue guang (Department of Chemistry, University of Science and Technology of China, Hefei 230026, China);Determination of Tetracyclines Antibiotics by Reversed-Phase High Performance Liquid Chromatography[J];Chinese Journal of Chromatography;2002-01
2 JIA Wei, SUN Lu, SHI Xiang guo, CHEN Xiao yan, ZHONG Da fang (Laboratory of Drug Metabolism and Pharmacokinetics, Shenyang Pharmaceutical University, Shenyang 110016, China);Measurement of the four tetracycline residues in the milk by high-performance liquid chromatography mass spectrometry[J];Journal of Shenyang Pharmaceutical University;2002-02
3 CHEN Yu _ fang(Guangzhou Exit-Entry Inspection & Quarantine Bureau, Guangzhou 510623, China);Determination of Tetracyclines Residues in Animal Muscle Tissues by SPE-HPLC[J];Journal of Instrumental Analysis;2003-03
Chinese Journal Full-text Database 10 Hits
1 FENG Yu1,SHENG Xuan2,ZHENG Ping2,SUN Hao2,YANG Yan-yan2 (1.Anhui Chlor-Alkali Chemical Group Co.Ltd.,Hefei 230011,China; 2.Anhui Entry-Exit Inspection and Quarantine,Hefei 230061,China);Research Progress on Avermectins Residues Analysis[J];Anhui Chemical Industry;2008-01
2 PAN Xiao-cheng et al (Anhui Agricultural University,Hefei,Anhui 230036);Synthesis and Identification of Ofloxacin Artificial Antigen[J];Journal of Anhui Agricultural Sciences;2006-03
3 WANG Wei-hua et al(Henan Institute of Science and Technology,Xinxiang,Henan 453003);Application of ELISA in the Residue Determination of Sulfonamide[J];Journal of Anhui Agricultural Sciences;2006-06
4 SUN Ming-na et al (Key Laboratory of Crop Quality Amelioration in Anhui Province,Hefei,Anhui 230031);Study on the Development Method of Abamectin Residue Determination[J];Journal of Anhui Agricultural Sciences;2006-12
5 ZHANG Yin-zhi et al(National Key Lab of Food Science and Technology,Southern Yangtze University,Wuxi,Jiangsu 214036);Study of Rapid Detection on Tetracycline Antibiotics in Food by Using Gold-labeled Reagent Strip[J];Journal of Anhui Agricultural Sciences;2008-27
6 ZHAO Jian-ya et al(School of Public Health,Nantong University,Nantong,Jiangsu 226019);Uncertainty Analysis of β-agonists in Pork Liver by ELISA[J];Journal of Anhui Agricultural Sciences;2012-18
7 PEI Dao-guo 1 WAN Yu-ping 2 LI Jing 2 DU Xian-ming 1 LIU Qing-lin 1(1 Linyi Entry-Exit Inspection and Quarantine Bureau in Shandong Province,Linyi Shandong 276034;2 Beijing Wanger Bio-technology Corp.Limited);Study on Determination of Kananmycin in Animal Resources Food by ELISA Method[J];Modern Agricultural Sciences and Technology;2010-19
8 QI Ke-zong~1,ZHU Liang-qiang~2,XU Shi-fu~2,WANG Xue-yan~1,XING Yin-shou~1 (1.College of Animal Science and Technology,Anhui Agricultural University,Hefei 230036; 2.Anhui Provincial Control Institute of Veterinary Pharmaceuticals and Feed, Hefei 230022);Determination of Recovery Rates of Four Fluoroquinolones Residues in Chicken′s Liver by HPLC[J];Journal of Anhui Agricultural University;2005-01
9 ZHANG Dan-jun1,PAN Xiao-cheng1,CHENG Bao-yan1,ZHAO Rui-hong1,XU Shi-fu2,TANG Chun-lian2,SUN Jun-xia3,HU Xiao-miao1(1.Institute of Animal and Veterinary Science,Anhui Academy of Agricultural Science,Hefei 230031;2.Anhui Provincial Control Institute of Veterinary Pharmaceuticals and Feed,Hefei 230022;3.Tongling Zhenqiang Poultry Company,Tongling 244100);Development of HPLC method for determination of ofloxacin levels in excrements of chicken[J];Journal of Anhui Agricultural University;2009-01
10 Chen Yijun Liu Yongjun;Determination of 17 β-Estradiol、Estriol,Ethinylestradiol,Estrone in Infant Milk with Gas Chromatography-Mass Spectrometry[J];Beijing Agriculture;2012-12
China Proceedings of conference Full-text Database 10 Hits
1 He Danting Li Yanwei Shi Wei Zhao Ning Xu Fei;Research and Trait Identification of Colloidal Gold Strip for Rapid Detection of Enrofloxacin[A];[C];2011
2 Hu Haiyan~1 Zhu Mingwen~1 Hu Hao~2 1 China Institute of Veterinary Drug Control,Beijing,100081; 2 China Medicine Association,Beijing,100022;Status and Developmental Countermeasures about Control and Determination of Veterinary Drugs Residues in Animal Derived Foods[A];[C];2011
3 SUN Zhi-wen,YAN Xiao-feng (Beijing Institute of Veterinary Drug Control,Beijing 100107,China);Determination of Phenylethanolamine A with Liquid Chromatography-Tandem MassSpectrometry in Swine Muscle[A];[C];2011
4 WU Li-qin,XIAO Tian-an,DENG Guo-dong (Guangdong Institute for Veterinary Drug and Feedstuffs Control,Guangzhou 510230);Progress in the Analytical Methods of Ractopamine Residue[A];[C];2011
5 YAN Feng,ZHANG Wen-gang,LI Dan-ni,CAO Ying,JIANG Yin,HUANG Shi-xin (Shanghai Institute of Veterinary Drug and Feeds Control,Shanghai 201103,China);Determination of Fifteen Kinds of β-agonists in Feed by UPLC-MS/MS Method[A];[C];2008
6 SUN Lei,ZHANG Li,HUANG Yao-ling,WANG Xia,WANG Shu-huai (China Institute of Veterinary Drug Control,Beijing 100081,China);Determination of Streptomycin and Dihydrostreptomycin in Milk by LC-MS/MS[A];[C];2008
7 MA Qiang,WANG Chao,WANG Xing,BAI Hua,CUI Yan-ni,WU Ting, HE Rui-yun,WANG Yan-bin (Institute of Industrial Product Inspection,Chinese Academy of Inspection and Quarantine,Beijing 100123,China);Determination of 21 Sulfonamides in Cosmetics by HPLC and Verified by HPLC-MS[A];[C];2008
8 XIA Xi~(1,2),LI Xiao-wei~(1,2),JIANG Hai-yang~(1,2),LI Jian-cheng~(1,2),AN Bao-chao~1,DING Shuang-yang~(1,2) (1.College of Veterinary Medicine,China Agricultural University,Beijing 100193,China;2.China National Reference Laboratory for Veterinary Drug Residue,Beijing 100193,China);Determination of Four Macrolides in Pork by High Performance Liquid Chromatography-Tandem Mass Spectrometry[A];[C];2008
9 Chen Shuchi (College of Food,South China Agricultural University Guangzhou 510642,China);Application of immunoassay technology in the field of food detection[A];[C];2010
10 Wei Xinlin~1,Liu Ying~1,Zhang Shaoen~2,Wang Yuanfeng~1 (1.School of Life and Envirnoment,Shanghai Normal University,Shanghai 200234,China; 2.Nankai Biotechnology Limited company,Hangzhou,Zhejiang 310051,China);Synthesis and Identification of Fenvalerate Specific Artificial Antigen[A];Chinese Society of Agricultural Engineering[C];2009
Chinese Journal Full-text Database 10 Hits
1 ZHU Gui-fen et al(College of Chemistry and Environment Sciences,Henan Normal University,Xinxiang,Henan 453007);Enrichment Rules of Heavy Metals Cd and Ni in Brassica juncea Treated with EDTA[J];Journal of Anhui Agricultural Sciences;2007-11
2 YUAN Ke et al(Zhangjiagang Entry-Exit Inspection and Quarantine,Zhangjiagang,Jiangsu 215600);Comparative Study on Gold Labeled Strips and ELISA for Detection of DON[J];Journal of Anhui Agricultural Sciences;2007-18
3 DONG Yu-ying et al(Department of Environmental Engineering,Dalian Nationalities University,Dalian,Liaoning 116600);Environmental Trend,Harm and Prevention of Antibiotics in the Stockbreeding[J];Journal of Anhui Agricultural Sciences;2008-06
4 MA Su-ying et al(College of Pharmacy,Xinxiang Medicinal University,Xinxiang,Henan 453003);Determination of the Residues of Ciprofloxacin Hydrochloride in Eggs by HPLC[J];Journal of Anhui Agricultural Sciences;2008-26
5 ZHANG Yin-zhi et al(National Key Lab of Food Science and Technology,Southern Yangtze University,Wuxi,Jiangsu 214036);Study of Rapid Detection on Tetracycline Antibiotics in Food by Using Gold-labeled Reagent Strip[J];Journal of Anhui Agricultural Sciences;2008-27
6 CHI Li-min et al(Hebei Chemical and Pharmaceutical college,Shijiazhuang,Hebei 050026);Determination of Tetracycline Antibiotics in Meat by HPLC[J];Journal of Anhui Agricultural Sciences;2010-07
7 WANG Meng-chan et al(Department of Analytical Chemistry,China Pharmaceutical University,Nanjing,Jiangsu 210009);Effects of Chlortetracycline Hydrochloride and its UV Degradation Products on Growth of Freshwater Algae[J];Journal of Anhui Agricultural Sciences;2011-07
8 LI Yong xin, ZHAO Dan hua, ZHUO Shu jiuan, ZHU Chang qin, WANG Lun (The College of Chemical and Material Sciences,Anhui Normal University,Wuhu 241000, China);DETERMINATION OF TRACE AMOUNT OF LEAD BY THE RESONANCE LIGHT-SCATTERING METHOD[J];Journal of Anhui Normal University(Natural Science);2002-03
9 FANG Fang~1,ZHENG Hong~2,LI Ling~1,DIAO Xue-lian~1, XIA Yun-sheng~1,ZHU Chang-qing~(1)(1.College of Chemistry and Materials Science,Anhui Normal University, Wuhu 241000,China;2.Department of Chemistry,Xiamen University,Xiamen 361005,China);Determination of Anionic Surfactant by a Resonance Light-scattering Technique Using a Near-infrared Cationic Cyanine[J];Journal of Anhui Normal University(Natural Science);2006-02
10 MA Wan-zhu1 ZHANG Ming-kui 2(1 Institute of Environment Resources,Soil and Fertilizer,Zhejiang Academy of Agricultural Science,Hangzhou Zhejiang 310021;2Zhejiang Provincial Key Laboratory of Subtropical Soil and Plant Nutrition,College of Natural Resource and Environmental Sciences,Zhejiang University);Effect Research of Oxytetracycline on Microorganisms Number and Enzyme Activity in Soil Affected by Pig Manure[J];Modern Agricultural Sciences and Technology;2010-08
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 LI Chuang et al(College of Resource and Environmental Science,Jilin Agricultural University,Changchun,Jilin 130118);Determination of Pendimethalin,Oxyfluorfen and Acetochlor Residue in Garlic by GC[J];Journal of Anhui Agricultural Sciences;2011-22
2 TIAN Ye et al(Beijing Institute of Plant Nutrition and Resources,Beijing 100097);Migration Impact of Antibiotics in Organic Fertilizers on Soil and Plants[J];Journal of Anhui Agricultural Sciences;2012-08
3 Lin Jie,Huang Xiaorong,Zheng Jing,Chen Bin,Huang Changjiao;Rapid detection of β-lactams and tetracyclines residues in UHT milk by rosa method[J];Feed Industry;2011-07
4 NING Hai-rong1,PENG Ying2,JIN Xing-liang1,XIAN Shi-xiong1,XIE Chun-yan3(1.Animal and Plant Quality Inspection Center of Guangming New District,Shenzhen 518107,China;2.Hunan Network Engineening Vocational College,Changsha 410004,China;3.Xingjia Bio-engineering Co.,Ltd.,Changsha 410001,China);Research Progress of Detection Method of Antibiotics in Milk[J];China Animal Husbandry & Veterinary Medicine;2012-08
5 SUN Yan-hong,JIA Yan-xia,LIU Hai-ping,YAN Zao-ying,REN Yong-xia,ZHAO Hai-xiang(Hebei North University,Zhangjiakou,Hebei 075000);Effect of Common Antibiotics on the Sprouting and the Vigor of Three Vegetable Seeds[J];Northern Horticulture;2012-20
6 PU Ming et al(Changji Animal Products Quality Inspection Center,Changji,Xinjiang 831100);β-lactam Antibiotics and Tetracycline Antibiotic Two-Linked Test Strip Quality Verified Test[J];Journal of Anhui Agricultural Sciences;2012-31
7 ZHANG Ping1,2,Lü Xing-ping1,FAN Jun-min1,TIAN Tian1,LIU Jing-jing1,FAN Jin-shan1(1.Jiangsu Polytechnic College of Agricultural and Forestry,Zhenjiang,Jiangsu,212400,China; 2.Nanjing Agricultural University,Nanjing,Jiangsu,210095,China);Investigation on Residues of Antibliotics in Fresh and Raw Milk in Zhenjiang[J];Progress in Veterinary Medicine;2013-06
8 LI Yang1,2,HE Shun-qin2,XUE Jing-jiao2,CAO Jing-li2,HU Qiu-fen2(1.Center for Disease Control of Epidemic Prevention Station of Yunnan Province,Kunming 650022,China;2.College of Chemistry and Biotechnology,Yunnan Nationalities University,Kunming 650031,China);Determination of Chloramphenicol Residues in Milk by UPLC-MS/MS Method[J];Animal Husbandry and Feed Science;2010-08
9 YU Fang,ZHAO Jin-hui,LIU Mu-hua*(Optics-electrics Application of Biomaterils Lab,College of Engineering,JAU,Nanchang 330045,China);Detection of Chlortetracycline Residues in Milk Based on Three-dimensional Fluorescence Spectroscopy[J];Acta Agriculturae Universitatis Jiangxiensis;2012-04
10 WANG Wen-hui1,LIU Hui-yan2,WANG Yu-jue1,WANG Yue1,SHAO Fu-xiang1,ZHU Yong3,SUN Guo-xin1(1.Heilongjiang Entry-Exit Inspection and Quarantine Bureau,Harbin 150030,China;2.Heilongjiang Land Reclamation Dragon King Foods Co.Ltd.,Suihua 152000,China;3.Wanxiang Doneed Co.,Ltd,Harbin 150030,China);Study of rapid detection methods of antibiotic residue in raw milk[J];China Dairy Industry;2011-07
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 Liu Yan, Liu Mei, Yin Qiyou, et al (Institute of Neuroscience, Nantong Medical College, Nantong 226001);THE MEANS OF SCREENING cDNA LIBRARY BY DIG-LABLED PROBE AND PLAQUE HYBRIDIZATION[J];ACTA ACADEMIAE MEDICINAE NANTONG;1997-03
2 Zhao Jing , Yang Hanchun , Li Hua , Gao Yun , Chen Sheng , Zha Zhenlin (Col1ege of Veterinary Medicine,China Agricultural University,Beijing l00094);Detection of Kanamycin Resistance Gene for E.coli in Swine by PCR[J];JOURNAL OF AGRICULTURAL BIOTECHNOLOGY;2000-03
3 Xu Hongbing(Dept of Biochemistry,Wannan Medical College,Wuhu 241001);HYBRIDIZATION WITH BIOTINYLATED PROBE[J];JOURNAL OF WANNAN MEDICAL COLLEGE;1997-04
4 Yan Shifang Bao Youdi (Laboratory of Genetic Engineering, Fujian Medical College, Fuzhou);TWO BIOTIN-LABELED PROBES OF GENTAMICIN RESISTANCE GENES[J];Acta Microbiologica Sinica;1991-02
5 Chen Nanhui,Guo Minhong,Huang Gengming (Jiangxi Agricultural University) He Xiaoqing,Liu Xiaoling (Jiangxi Hygienic and Antiepidemic Station) Pan Ruonan,Wei Xulan,Luo Ming (Nanchang Institute of Medical sciences);BACTERIOPHAGE TYPING,ANTIBIOTIC SENSITIVITIES AND PLASMID ELECTROPHORESIS ANALYSIS OF SALMONELLA PULLORUM[J];ACTA VETERINARIA ET ZOOTECHNICA SINICA;1997-05
6 PAN zhiming,JIAO Xinan,LIU Xuexian,NI Zhenya,LIU Wenbo,GAO Song,ZHANG Rukuan,LIU Xiufan (College of Animal husbandry Veterinary Science,Yangzhou University,Yangzhou 225009,China);Changes of Drug Resistance of Salmonella Pullorum[J];CHINESE JOURNAL OF PREVENTIVE VETERINARY MEDICINE;1999-04
7 SHI Weimin(College of Veterinary Medicine, china Agricultural Uninersity, Beijing 100094, china);Detection of the Tetracycline Resistance Gene from E. coli by PCR[J];CHINESE JOURNAL OF PREVENTIVE VETERINARY MEDICINE;1999-06
8 Li Xue wu et al (Animal and veterinary institute,Henan Academy of Agricultural Scienas);Detection of Pseudorabies with Digoxin Labelled DNA Probe[J];;1997-03
9 Zhang Xiaolin,Wang Fu,Zhu Demei. Institute of Antibiotics,Huashan Hospital,Shanghai Medical University,Shanghai 200040;The investigation of outer membrane barrier mechanism in multiple antibiotic resistant Escherichia coli[J];CHINESE JOURNAL OF INFECTIOUS DISEASES;1998-04
10 Sun Xianfeng,Liu Xiaoxia.Department of Microbiology,Suzhou Medical College,Suzhou 215007;The detection and location of drug resistant gene in Salmonella typhi[J];CHINESE JOURNAL OF INFECTIOUS DISEASES;1998-04
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved