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《Journal of Anhui Agricultural Sciences》 2008-05
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Study on Organophosphorus Pesticide Residue in Chinese Medicinal Material

SUI Wu-bin(Department of Chemistry,Zaozhuang University,Zaozhuang,Shandong 277101)  
[Objective] A high performance gas chromatorgraphic method was developed to determine the content of 8 organophosphorus pesticides residues in Hyoscyamus niger L.,Rhizoma Pinelliae Cortex,Eucommia ulmoides Oliv.,Evodia rutaecarpa(Juss.)Benth,Gastrodia elata,Cynanchum bungei Decne.[Method] The organophosphorus pesticides residues were analyzed by employing a fused silica capillary column DB-35 at the operating conditions of column temperature,flame photometric detector(FDT),nitrogen,taking air,H2 as carrier gas.[Result] Eight organophosphorus pesticides residues were separated.The calibration curve of 8 organophosphorus pesticides residues was linear in the range of 1~100 ng/ml(r0.9999).The detective limit range was 0.021~0.100 μg/ml.The average recovery was 81 %~95 %.[Conclusion] The method was sensitive and reliable to determine the organophosphorus pesticides residues of Chinese medicinal material.
【Fund】: 枣庄市科技局科技攻关资助项目(No:200538)
【CateGory Index】: S481.8
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Chinese Journal Full-text Database 3 Hits
1 BAN Rui et al(College of Chemistry and Environmental Science,Guizhou University for Nationalites,Guiyang,Guizhou 550025);Study on Multiresidue Determination of Organochlorine and Pyrethroid Pesticides in Tea by Gas Chromatography[J];Journal of Anhui Agricultural Sciences;2009-04
2 LI Fu-hou et al(Key Laboratory of Marine Biotechnology of Jiangsu Province,School of Marine Science and Technology,Huaihai Institute of Technology,Lianyungang,Jiangsu 222005);Research Progress on Microbial Degradation of Organophosphorus Pesticides[J];Journal of Anhui Agricultural Sciences;2009-22
3 WU Long,ZENG Wen-fang,YANG Zhong-qiao,JIN Quan(Hangzhou Center for Disease Control and Prevention,Hangzhou 310006,China);Determination of fifteen kinds of organophosphorus pesticides in a Chinese traditional medicine by gas chromatography[J];Chinese Journal of Health Laboratory Technology;2009-02
Chinese Journal Full-text Database 10 Hits
1 ZHAO Er-Cheng et al(Chinese Agricultural University,Beijing 100094);Research Advance in the Residue Analysis of Plant Growth Regulator[J];Journal of Anhui Agricultural Sciences;2005-09
2 SUI Wu-Bin(Department of Chemistry,Zaozhuang College,Zaozhuang,Shandong 277101);Study on the Determination Method of the Residual Quantity of Multi-Organophosphorus Pesticides in Honey[J];Journal of Anhui Agricultural Sciences;2007-29
3 Li Shuang1,Du Wei2,Li Shoufu1(1.Heilongjiang Environmental Protection Research Institute,Harbin 150056,China; 2.Dongning Environmental Monitoring Station,Dongning 157200,China);Determination of Trichlorfon Residues in Water by Pyrolysis Gas Chromatography[J];Environmental Science and Management;2009-07
4 HUANG Hong-lin, LIU Shi, ZHANG Tao-zhi~* (Center of Testing and Analysis, Central China Normal University, Wuhan 430079);Determination of Gibberellin Residue in Tomato by Solid Phase Extraction-High Performance Liquid Chromatography[J];Journal of Analytical Science;2005-01
5 LIU Yong*,YANG Chang-zhi and KANG Qing-he(Technology Center of Heilongjiang Entry-Exit Inspection and Quarantine Bureau,Harbin 150001);Determination of trichlorfon residues in foodstuffs of animal origin by pyrolysis gas chromatography[J];Chinese Journal of Analysis Laboratory;2008-02
6 JIANG Ting,ZHANG Guo-wen* and WANG An-ping(Key Laboratory of Food Science of Ministry of Education,Nanchang University,Nanchang 330047);Study on interaction of bromocresol green-triton X-100 with prometryne by resonance light scattering measurements[J];Chinese Journal of Analysis Laboratory;2008-06
7 PENG Jing-He HUANG Gao-Ling ZHANG Yong ZHU Ya-Xian a (Key Laboratory of Marine Environmental Science of MOE,Xiamen University,Xiamen,Fujian 361005,P.R.China) a(Department of Chemistry,Xiamen University,Xiamen,Fujian 361005,P.R.China);Room Temperature Phosphorescence of Carbaryl Induced by β-Cyclodextrin in the Presence of Heavy Atom Perturbation[J];Chinese Journal of Spectroscopy Laboratory;2004-04
8 SONG Zheng-ping,TIAN Shi-long,WANG Dong-hui,ZHU You-chun(Testing Center,Gansu Academy of Agricultural Sciences,Lanzhou 730070,China);An Analytical Study on Organophosphorus and Carbamate Pesticide Residues in Vegetables by GC-TSD[J];Journal of Gansu Sciences;2006-02
9 ZHANG Yan(The Supervision and Testing Center for Lycium Quality,Ministry of Agriculture,Yinchuan Ningxia 750002,China);Evaluation Different Extraction Solvent in Analysis of Pesticide Residues[J];Gansu Agricultural Science and Technology;2006-09
10 HAN Yan1,2 (1.State Key Laboratory of Marine Environmental Science,Environmental Science Reasearch Center, Xiamen University,Xiamen Fujian 361005,China; 2.School of Chemistry and Chemical Engineering,Fuyang Teachers College,Fuyang Anhui 236032,China);Simultaneously determination of some organophosphorus pesticide residues in vegetables[J];Journal of Fuyang Teachers College(Natural Science);2009-02
Chinese Journal Full-text Database 10 Hits
1 HUANG Xiao-mei et al (College of Resources and Environmental Sciences,Xinjiang Agricultural University,Urumqi,Xinjiang 830052);Influence of Organic Phosphorous Pesticides on Soil Respiration[J];Journal of Anhui Agricultural Sciences;2007-07
2 LI Jian-jun et al(Weifang Entry-exit Inspection and Quarantine Bureau,Weifang,Shandong 261041);Discuss on Determining Methods of Pesticide Residue in Vegetable and its Products[J];Journal of Anhui Agricultural Sciences;2007-33
3 ZHOU Gang et al(College of Plant Protection,Southwest University,Chongqing 400716);Research Progress on the Pyrethroid Pesticide Residue Degradation Dynamics in Farm Produce[J];Journal of Anhui Agricultural Sciences;2008-05
4 YANG Sheng-quan et al(College of Resource and Environment,Southwest University,Chongqing 400716);Methods of Decomposing Pesticide Residues from Vegetable and Fruit[J];Journal of Anhui Agricultural Sciences;2008-06
5 ZHAO Si-qi et al (College of Life Science and Biopharmaceutics,Shenyang Pharmaceutical University,Shenyang,Liaoning 110016);On the Detection Technologies of Pesticide Residues[J];Journal of Anhui Agricultural Sciences;2008-10
6 YAO Jie et al(The National Center of Agricultural Standardization and Supervision(Anhui),Hefei,Anhui 230051);Degradation Lapse of Two Organophosphorus Pesticides in the Environment[J];Journal of Anhui Agricultural Sciences;2008-11
7 GAO Qian et al(Key Lab of Agr-food Safety of Anhui Province,College of Resource and Environment,Anhui Agricultural University,Hefei 230036);Research Status of the Pesticide Residue in Chinese Herbal Medicine[J];Journal of Anhui Agricultural Sciences;2008-23
8 Liu Yunhuan 1,Chen Donghai 2 (1.2HenanUniversity Of Technology,Zhengzhou 450052 );Study Progress on Microbial Degradation of Organophosphates[J];North Environment;2005-01
9 DONG JinBin1 WANG JinHua2 LU XiaoYu2 XU ChaoYi2 YANG JunJiao1 (1.School of Science,Beijing University of Chemical Technology,Beijing 100029; 2.Beijing Entry-Exit Inspection and Quarantine Bureau Technology Centre,Beijing 100026,China);Multi-residue determination of 42 pesticides in tea by gas chromatography-mass spectrometry[J];Journal of Beijing University of Chemical Technology(Natural Science Edition);2007-05
10 Zheng Hong,Tang Mingqiang(Department of Biology and Chemistry Engineering,Fuqing Branch of Fujian Normal University,Fuqing,350300);Advance of Studies on Microbial Degradation of Organophosphorus Pesticides[J];Journal of Fuqing Branch of Fujian Normal University;2008-02
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