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《Journal of Anhui Agricultural Sciences》 2009-14
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Study on Extracting Total Flavonoids from Hypericum perfortum L. with Microwave-assisted Extraction

WANG Xiao-hua et al(Department of Chemistry and Life Science,Xiangnan University,Chenzhou,Hunan 423000)  
[Objective] The study aims to discuss the optimum technological conditions of extracting total flavonoids from Hypericum perfortum L.with microwave-assisted extraction.[Method] Microwave power,extraction solvent concentration,liquid-solid ratio,and extraction time are investigated and the appropriate microwave-assisted exteaction conditions are obtained with the orthogonal test method.The microwave-assisted exteaction method is compared with ultrasonic extraction and soxhlet extraction methods.[Result] The optimized conditions of microwave-assisted extraction are as follows: ethanol concentration is 70 %,liquid-solid ratio is 30∶ 1,microwave power is 450 W,and extraction time is 5 minutes.Also the extracting yield of flavoniods from Hypericum perfortum L.is up to 6.02 % under the optimal extraction conditions.The yield of total flavonoids is almost equal to soxhlet extraction method for 4 hours,and ultrasonic extraction method for 1 hours.[Conclusion] The microwave-assisted extraction method is a fast,efficient,energy saving and high-selective.
【Fund】: 湖南省自然科学基金资助项目(07JJ3017);; 湖南省教育厅优秀青年科研基金项目(06B089)
【CateGory Index】: R284.2
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【References】
Chinese Journal Full-text Database 6 Hits
1 Liu Jianxiang,Jiang Jie,Wei Zhengxi(School of Medicine and Life Sciences,Zhejiang University City College,Hangzhou 310015,China);Extraction and Purification of Total Flavonoids from SJW[J];Guangdong Chemical Industry;2010-12
2 FENG Jun-jiao et al(College of Life Science,Shaanxi Normal University,Xi'an Shaanxi 710062);Establishment and Condition Optimization of ISSR-PCR Amplification System of Hypericum perforatum Linn.[J];Journal of Anhui Agricultural Sciences;2012-36
3 JIANG Bo1,2,YE Jie2,ZHOU Zhang-zhang2,XIE Gan2,HUANG Si-di2,ZHAO Zheng-yu2,LV Hong-fei2 1.College of Biology and Food Engineering,Changshu University of Science and Technology,Changshu,Jiangsu 215500,China;2.College of Chemistry and Life Science,ZheJiang Normal University,Jinhua,Zhejiang 321004,China;Effects of Cycocel on Growth and Hypericin Content of Hypericum perforatum L[J];药用植物研究(英文版);2010-08
4 SHANG Xi-li*,WEI Yong-xiang Department of Chemistry and Engineering,Binzhou University,Binzhou,Shandong 256600,China;Isolation,Purification and Components Analysis of Polysaccharide from Wild Lycium barbarum of Shandong Province[J];药用植物研究(英文版);2010-09
5 KUANG Chao-yang,OUYANG Yu-zhu,CHEN Shi(College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000,China);Optimization on Extraction Technology of Flavonoids from the Forsythia by Water-enzyme Hydrolysis Synergism Ultrasonic[J];Food and Fermentation Technology;2012-01
6 SHA Kun1,ZHANG Ze-jun2(1.China Agricultural University(Yantai),Yantai 264670;2.College of Food Science and Nutritional Engineering,China Agricultural University,Beijing 100083);Study on extraction of psoralen from Ficus carica leaves by microwave-assisted method[J];Food Science and Technology;2010-08
【Citations】
Chinese Journal Full-text Database 8 Hits
1 HU Dong-hua1,GAO Ying1,SHAO Chen2,FENG Qian-kun1,WANG Rui3(1.Traditional Chinese Medicine Collage of Changchun,Changchun 130017,China;2.Department of Chemistry,Northeast Normal University,Changchun 130024,China;3.Institute of Geological Science,Changchun 130012,China);Studies on Hypericin in Hypericum perforatum L and it's interactions with HIV-1 Rt[J];Journal of Molecular Science;2008-04
2 Liang Yan,Ying Miaomiao,Lü Yinghua,Lu Xianying,Zhang Ying~※(College of Biosystem Engineering and Food Science,Zhejiang University,Hangzhou 310029,China);Microwave-assisted technology for extracting Opuntia polysaccharide[J];Transactions of the Chinese Society of Agricultural Engineering;2006-07
3 ZHAO Gong ling LOU Tian jun ZHAO Da ke GUO Yan ming (Henan Vocation Technical Teachers' College, Xinxiang, Henan 453003,China);Study on extractive technology of lycopene by microwave radiation and enzyme[J];Food and Machinery;2004-01
4 LU Li-shuang PAN Dao-dong(Department of Food Science and Technology,Jinling College, Nanjing Nomal University,Nanjing,Jiangsu 210097,China);The influence of microwave on the extraction of oligomeric proanthocyanidins from grape seed[J];Food and Machinery;2004-06
5 LiRong et al;New Technology on Microwave Extraction of Ginkgo Biloba Flavone Glycosides[J];FOOD SCIENCE;2000-02
6 CHEN Wei1,2,LIU Qing-mei1,*,YANG Xing-min1,YU Zhi-fang2,YING Min1 (1.Ningbo Key Laboratory of Agricultural Products Processing Technology, Zhejiang Wangli University, Ningbo 315100, China;2.Department of Food Science, Nanjing Agricultural University, Nanjing 210095, China);Study on the Extraction Technology Microwave of Flavonoids from Eucommia[J];Food Science;2006-10
7 ZHANG Meng jun, JIN Jian feng, LI Bo yu, LI Zhi liang (College of Chemistry and Chemical Engineering, Chongqing University, Chongqing 400044, China);Study of Microwave-assisted extraction on flavonoids of Radix Glycyrrliza[J];Chinese Traditional Patent Medicine;2002-05
8 YIN Zhi Qi, YE Wen Cai, ZHAO Shou Xun Department of Phytochemistry, China Pharmaceutical University, Nanjing 210038, China;Studies on Chemical Constituents from Hypericum perforatum of China Origin[J];Journal of China Pharmaceutical University;2002-04
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 RAN Xu et al (Department of Food Science and Engineering, Sichuan University, Chengdu, Sichuan 610065);Study on Microwave-assisted Extraction Technology of Total Flavonoids from Kuding Tea[J];Journal of Anhui Agricultural Sciences;2008-21
2 XIA Min(Instrumental Analysis Center,Chemical Department,Huaiyin Teachers College,Huaian,Jiangsu 223300);Study on the Extraction Conditions of Solanesol from the Unusable Shredded Tobacco[J];Journal of Anhui Agricultural Sciences;2008-35
3 FU Wen-qun et al (Department of Biological Sciences and Biotechnology,Zhangzhou Normal University,Zhangzhou,Fujian 363000);Study on the Microwave-assisted Extraction of Flavonoids from Hedyotis diffusa Willd[J];Journal of Anhui Agricultural Sciences;2009-30
4 HUANG Yun-hong et al(College of Life Science,Jiangxi Normal University,Nanchang,Jiangxi 330022);Study on the Technology of Extracting Flavonoids from Orange Peel by Microwave Method[J];Journal of Anhui Agricultural Sciences;2010-04
5 LI Yun-he et al (Cancer Center,Sun Yat-sen University,Guangzhou,Guangdong 510060);Comparison of Hypericin Contents in Hypericum hubeiense and Hypericum perforatum[J];Journal of Anhui Agricultural Sciences;2010-28
6 LIU Yan et al(Department of Chemistry,Zunyin Normal College,Zunyi,Guizhou 563002,China);Study on the Effect of Different Extraction Methods on Rutin and Quercetin in Rosa laevigata Michx[J];Journal of Anhui Agricultural Sciences;2011-08
7 FENG Ji-nan et al(Department of Chemistry and Life Science,Xiangnan University,Chenzhou,Hunan 423000);Microwave-assisted Extraction of Total Flavonoids from Hippophae rhamnoides L[J];Journal of Anhui Agricultural Sciences;2011-26
8 LI Hao et al(Science Technology Department,Maanshan Teacher's College,Maanshan,Anhui 243041);Optimization of the Microwave-assisted Extraction Process of Polysaccharides from FRUCTUS CORNI[J];Journal of Anhui Agricultural Sciences;2011-26
9 XU Ya-wei,YU Xiao-ming,ZHANG Xin(Jilin Agricultural Science and Technology College of Bioengineering,Jilin,Jilin 132101);Study on Extracting Procedure of Proanthocyandins from Water Wax Trees Fruit[J];Northern Horticulture;2010-22
10 Gao Hegang,Ye Yong,Hu Aixi Pharmaceutical Engineering Department,School of Chemical and Energy Engineering,South China University of Technology,Guangzhou(510640);Antitumor Mechanism and Preparative Method of Phenolic Compounds in Traditional Chinese Medicine[J];Journal of Zhejiang University of Traditional Chinese Medicine;2007-05
China Proceedings of conference Full-text Database 3 Hits
1 YU Lei,LIU Shao-song,HAO Peng-fei,YANG Yun(Henan University of TCM,Zhengzhou 450008,Henan,China);Study on the Enzyme Extraction Process of Hypericin[A];[C];2011
2 XU Zhi-hong,LI Lei,WU Fa-wen,TAN Shu-juan,PENG Jing,ZHANG Zhi-bing Department of Chemical Engineering,Nanjing University,Nanjing 210093,China;The Application of the Modified PVDF Ultraffltration Membranes in further Purification of Ginkgo Biloba Extraction[A];[C];2005
3 Lü Rui,YANG Jing,MU Xiao-jing,XIA Zhi-ning~* and FU Xiao-hong(Department of Pharmaceutics Institute of Chemistry and Chemical Engineering,Chongqing University,Chongqing 400030);Microwave-assisted extraction and content determination of polysaccharide in the pinellia[A];[C];2009
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 HUANG Guang-yuan et al(College of Gardening and Horticulture,Yangtze University,Jingzhou,Hubei 434025);Preliminary Study on the Application of CCC on Zoysia matrella Merr.[J];Journal of Anhui Agricultural Sciences;2006-05
2 XIAO Lin et al (Chemistry and Chemical Engineering School,Shanghai Jiaotong University,Shanghai 200245);Application of Enzyme Method for Extracting Botanic Ingredient[J];Journal of Anhui Agricultural Sciences;2006-08
3 CHEN Chun-gang et al (College of Food Science,Henan Institute of Science and Technology,Xinxiang,Henan 453003);Research and Application of Bio-flavonoids[J];Journal of Anhui Agricultural Sciences;2006-13
4 XU Hao(Department of Biological Science and Engineering,Shaanxi University of Technology,Hanzhong,Shaanxi 723001);Study on Chemical Compositions and Pharmacological Effect of Hypericum perforatum L.[J];Journal of Anhui Agricultural Sciences;2007-14
5 MIN Yong et al(Department of Chemistry,Honghe University,Mengzi,Yunnan 661100);Isolation and Determination on Two Lignans from the Seeds of Punica granatum[J];Journal of Anhui Agricultural Sciences;2007-23
6 HU Shang-lian et al (College of Life Science and Engineering, Southwest University of Science and Technology, Mianyang, Sichuan 621002);Effects of GA_3 and IAA on the Dynamic Accumulation of Flavonoid Content in Neosinocalamus affinins[J];Journal of Anhui Agricultural Sciences;2008-08
7 HUANG Xiao-dong et al(Institute of Educational Science,Quanzhou Normal College,Quanzhou,Fujian 362000);Study on Microwave-alkali Water Extraction Technics and Dynamic Content of Total Flavonoids in Syzyginm buxifolium Leaves[J];Journal of Anhui Agricultural Sciences;2008-11
8 LIU Jin-xiang et al(Key Laboratory of Food Science,Ministry of Education,Nanchang University,Sino-German Joint Research Institute,Nanchang,Jiangxi 330047);Study on Total Ginkgo biloba Flavonoids Etraction with Alkali-Solution and Acid-Isolation[J];Journal of Anhui Agricultural Sciences;2008-26
9 LIU Shi-wang et al (College of Life Science and Engineering,Huanggang Normal University,Huangzhou,Hubei 438000);Primary Discussion on the Hemostatic Activity of Aqueous Extracts from the Leaves of Eclipta prostrata L.[J];Journal of Anhui Agricultural Sciences;2008-31
10 FENG Pei-yong et al(College of Life Science of Ludong University,Yantai,Shandong 264025);Selection of the High-yielding Cellulose-niger Strain[J];Journal of Anhui Agricultural Sciences;2008-36
【Secondary References】
Chinese Journal Full-text Database 7 Hits
1 CAO Hong-bin,SHEN Ming-jin*,CHEN Lian-hui(Department of Chemistry,North Sichuan Medical College,Nanchong 637000,China);Application of Microwave Extraction in Chinese Traditional Medicine[J];Guangzhou Chemistry;2013-01
2 ZHUANG Yi-jun,ZHANG Yin(Department of pharmacy,The second hospital Offiliated to Fujian Medical University Quanzhou 362000,China);Medical research progress on Ficus carica leaves[J];Strait Pharmaceutical Journal;2011-12
3 HUANG Dan-dan;ZHANG Yin;Department of pharmacy,The Second Affiliated Hospital of Fujian Medical University;;Medical research progress on Ficus carica[J];Strait Pharmaceutical Journal;2013-12
4 Yueqiao CAO;Heng ZHANG;Peng XIONG;School of Life Science and Chemical Engineering Huaiyin Institute of Technology;Jiangsu Provincial Engineering Laboratory for Biomass Conversion and Process Integration;;Application of Cellulase-assisted Method to Extract Flavonoids from Plants[J];农业科学与技术(英文版);2014-05
5 KUANG Chao-yang,OUYANG Yu-zhu,CHEN Shi,ZHANG Ci-hai(College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000,China);Optimization on separation technology of the quercetin from the Forsythia by ion precipitation methods with response surface methodology[J];Applied Chemical Industry;2012-05
6 Wang Lei Zhang Zide Zhang Xiaona Ma Junlian * (College of Food Science and Technology, Agricultural University of Hebei, Baoding 071001, Hebei);Effects of 1-MCP Treatment on Ethylene Biosynthesis Metabolism of Fig Fruits during Storage[J];Journal of Chinese Institute of Food Science and Technology;2013-04
7 SHI Xue-ping;WU Liang-liang;Department of Engineering and Technology of Jiangsu Institute of Economic & Trade Technology/Jiangsu Food Safety Engineerning Research and Development Center;Nanjing Institute for Comprehensive Utilization of Wild Plant;;Simultaneous Determination of Four Flavonoids in Apocynum venetum Gathered in Different Seasons by High Performance Liquid Chromatography[J];Journal of Food Science and Biotechnology;2013-10
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 DING Ru Xian, XU Tie Feng, ZHANG Han Ming (Department of Pharmacognosy, College of Pharmacy, Second Military Medical University, Shanghai 200433, China);Tissue culture and rapid regeneration of Hypericum perforatum[J];Academic Journal of Second Military Medical University;2000-10
2 LI Cui qin,WANG Zhe zhi (Institute of Life Science,Shaanxi Normal University,Xian 710062,China);Studies on the choice of conditions for the extraction of hypericin from Hypericum perforatum[J];Acta Botanica Boreali-occidentalia Sinica;2001-06
3 GUO Xiao-wu~1,JI Xiao-qin~2(1 Applied Acoustics Institute,Shaanxi Normal University,Xian 710062,China;2 Department of Food Engineering,Shaanxi Normal University,Xian 710062,China);Studies on ultrasonic extracting technology of flavonoid compound in Eucommia ulmoides[J];Acta Botanica Boreali-occidentalia Sinica;2003-11
4 ZHAO Li-hui1,YU Xiang-hui2,JIANG Chun-lai2,WU Yong-ge2,SHEN Jia-cong2,KONG Wei2 (1.Collge of Life Science and Technology,Changchun University of Science and Technology,Changchun 130022,China;2.College of Life Science,Jilin University,Changchun 130012,China);Construction of HIV-1 envelope glycoprotein in Pichia pastoris[J];Journal of Molecular Science;2007-03
5 ZHOU Yi-han,LI Ze-sheng,HAN Wei-wei,YAO Yuan(Institute of Theoretical Chemistry,Jinlin University,Changchun 130023,China);Homology modeling and docking studies of homoserine transsuccinylase from Escherichia coli[J];Journal of Molecular Science;2008-02
6 Cui Yihua Cui Yingde Yi Guobin (Faculty of Chemical Engineering and Light Industry GDUT., Guangzhou 510090);Widely Application and It's Extraction Methods of the Natural Polysaccharide[J];Guang Zhou Chemical Industry and Technology;2002-03
7 YAN Zan-kai, LIU Chun-ying (Department of Environment Engineering , Hubei Agricultural College ,Jingzhou, Hubei 434025,China);Extraction Technology of Polysaccharides from Opuntia Milpa Alta[J];Journal of Hubei Agricultural College;2003-04
8 Zhang,Li Xue Ding,Jin Chang Gu,Heng Jie (Department of Chemistry,Wenzhou Teachers College,Wenzhou,325003);Application of Microwave Technique to Organic Synthesis[J];CHINESE JOURNAL OF SYNTHETIC CHEMISTRY;1996-01
9 Gong Sheng-zhao Yang Zhuo-ru(College of Chemical & Energy Engineering, South China Univ. of Tech., Guangzhou 510640,Guangdong,China);Investigation into the Microwave-assisted Extraction Technology for Astragalus Polysaccharide[J];Journal of South China University of Technology(Natural Science);2004-08
10 DENG Yu 1,YANG Yan 2,LU Hai yan 1,ZHANG Wei qiang 1 (1. Dept.of Chemical Engineering, Tianjin Univ. of light industry,Tianjin 300222;2.Third hostapil ,Tianjin Univ. of Medical Sciences, Tianjin 300203.);PRIMARY STUDY ON THE EXTRACTION OF LYCOPENE[J];Science & Technology In Chemical Industry;2002-01
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