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《Journal of Anhui Agricultural Sciences》 2011-10
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Multi-walled Carbon Nanotubes Surface O-dichlorobenzene Preparation of Molecularly Imprinted Polymers

WANG Jun et al(Geography and Environmental Science,Northwest Normal University,Lanzhou,Gansu 730070)  
Multi-walled carbon nanotubes grafted carbon-carbon double bond,to o-dichlorobenzene as a template for the function of styrene monomer:ethylene-glycol dimethacrylate as crosslinker by precipitation polymerization in surface of carbon nanotubes were successfully prepared o-dichlorobenzene imprinted materials by infrared spectroscopy,thermal analysis,scanning electron microscopy and transmission electron microscopy to characterize the material properties.The results show that the surface of carbon nanotubes grafted a layer of stable,uniform 30-50 nm thickness of the imprinted materials.High performance liquid chromatography to study the adsorption kinetics of imprinted materials and adsorption capacity,the results show that imprinted materials adsorption equilibrium time was 100 min,by Scatchard analysis,this polymer with o-dichlorobenzene has two binding sites,maximum adsorption capacity of 92.732 mol/g,equilibrium constant of 17.986 mol/L,more data and experiments show that this material can be successfully used to detect the environment,o-dichlorobenzene in the pre-treatment.
【CateGory Index】: TB383.1
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