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《Journal of Anhui Agricultural Sciences》 2011-12
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Determination and Isolation of the Nitrophenol Isomers in Well Water with Dual-Cloud Point Extraction and Capillary Electrophoresis

CHENG Jia et al(Key Laboratory for Drug Quality Analysis and Control of Hebei Province,College of Pharmacy,Hebei University,Baoding,Hebei,071002)  
[Objective] The reference for the determinate of the nitrophenol isomers in well water provided through the research.[Method] The material from well water was pretreatment with Dual-Cloud Point Extraction and measured with Capillary Electrophoresis.[Results] In the optimum condition,which concentration of the surfactant Triton X-114 was 0.5%,the pH was 1.5,the adding amount of NaCl was 0.020 g/ml,meanwhile,the adding amount of 0.2 mol/L NaOH was 100 μl,the nitrophenol isomers in well water were tested with the method of Dual-Cloud Point Extraction and Capillary Electrophoresis at the temperature of 40 ℃ for 20 minutes.There was good linearity between O-nitrophenol and M-nitrophenol in the range of 0.000 2-0.005 0 mg/mL,the recovery of the technique reached 97% and the relative standard deviation was less than 5%.[Conclusion] The result from the technique was accurate and environment-friendship because the effect of the surfactant in the accumulation phase on the isolation of capillary electrophoresis was eliminated.
【CateGory Index】: X832
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