Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Journal of Anhui Agricultural Sciences》 2014-29
Add to Favorite Get Latest Update

Research of Application in Sample Preparation Technology for Infrared Spectrum

WEN Ji-chang;WANG Jia-feng;Zhongjia Test Center of Guizhou Ltd.;  
The research aimed to select the appropriate sample preparation method. [Method]The sample of conventional sampling method——solid samples of KBr pressed method and KCl pressed method,and liquid samples of removable liquid cell method were described,and the advantages and disadvantages of these methods were compared at last. A modified method as for the disadvantages of pressed method had been put forward: impregnation,which was made by blank KBr tablet for film base. [Result]As for solid samples which could be dissolved in volatile organic solvents,this method could be used. And for high boiling point of liquid samples,the samples could be diluted by volatile organic solvents,then sampled by impregnation,in the other words,which was sampled after the blank KBr tablet with diluted organic solvent evaporated under the condition of infrared light. [Conclusion] Through comparison with the conventional pressed method-KBr pressed method,infrared spectrum of this modified preparation method could achieve the request of qualitative analysis,and made up the deficiency of conventional pressed method.
【CateGory Index】: S121
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 7 Hits
1 HE Xu-yuan~1 CHEN Yuan-dou~2 CAI Xiang-wen~1 CHEN Qi~1 (1.Department of Chemistry,Hunan University of Arts and Sience,Changde Hunan,415000;2.Changde Cigarette Factory,Changde Hunan,415000);Sampling Technology for Infrared Spectroscopy Based on Pure KBr Discs[J];Journal of Hunan University of Arts and Science(Natural Science Edition);2006-02
2 FAN Xue-fang,XU Miao,HOU Xiao-tao,WANG Shuai,LI Hong-yu,ZHANG Li-hua(School of Pharmacy,Beihua University,Jilin 132013,China);Infrared spectrum technology and its applications[J];Journal of Chengdu Medical College;2009-03
3 Shi Liang;Ding Jia (Hefei Economy and Technology College, Hefei, 230052);Problems in sample preparation for IR spectroscopic analysis and methods for their resolution[J];ANALYTICAL INSTRUMENTATION;1999-04
4 LIN De-Juan YOU Xiu-Li (Department of Chemistry,Zhangzhou Teachers College,Zhangzhou,Fujian 363000,P.R.China);Preparation Technique of Sample Solid Analysed by FTIR[J];Chinese Journal of Spectroscopy Laboratory;2003-01
5 CHEN Yun,SHI Zhen-zhi,XU Ke-xin,CHEN Wen-liang State Key Lab of Precision Measuring Technology and Instruments,Tianjin University,Tianjin 300072,China;Study on Temperature Correction of Near-Infrared Spectra of Solution[J];Spectroscopy and Spectral Analysis;2009-11
6 ZHU Lei, SU Yan (The 59th Research Institute of China Ordnance Industries,Chongqing,400039);Application of Fourier Transform Infrared Spectroscopy(FTIR) Analysis in Environmental Testing[J];Environmental Technology;2002-03
7 WU Han-fu (Department of Chemistry,Liupanshui Teachers College,shuicheng, 553004,China);Application of Infrared Spectroscopy[J];Journal of Liupanshui Teachers College;2006-03
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 LIANG Qi-feng et al (Department of Chemistry,Jiaying University,Meizhou,Guangdong 514015);Identification of the Honey Quality with the Technique of Infrared Spectrum[J];Journal of Anhui Agricultural Sciences;2009-01
2 HE Xu-yuan~1 CHEN Yuan-dou~2 CAI Xiang-wen~1 CHEN Qi~1 (1.Department of Chemistry,Hunan University of Arts and Sience,Changde Hunan,415000;2.Changde Cigarette Factory,Changde Hunan,415000);Sampling Technology for Infrared Spectroscopy Based on Pure KBr Discs[J];Journal of Hunan University of Arts and Science(Natural Science Edition);2006-02
3 LI Hong-yu,ZHANG Li-hua,YUAN Guang-xin,WANG Ming-ke (School of Pharmacy,Beihua University,Jilin 132013,China);Research on infrared fingerprint of Niuhuangjiedu pill[J];Journal of Chengdu Medical College;2010-01
4 ZHANG Jun-ying, GU Xiao-yu and CAI Xiao-xia(Beijing University of Chemical Technology, College of Material Science and Engineering,Beijing 100029);Quantitative investigation on preparation method of testing sample for studying curing keinetics of epoxy resin by FTIR[J];Analytical Laboratory;2005-09
5 SUN Shu-Qing JIANG Chuan-Fu LIU Qian-Chong (Department of Chemistry,Bohai University,Jinzhou,Liaoning 121000,P.R.China);Preparation Technique of Vapor Sample of Volatile Liquid for FTIR Analysis[J];Chinese Journal of Spectroscopy Laboratory;2004-03
6 LI Xiao-hong,JIANG Xiang-ping*,CHEN Chao,TU Na Jingdezhen Ceramics Institute,Jingdezhen 333001,China;Research on Diffuse Reflectance Infrared Fourier Transform Spectroscopy of Kinds of Kaolin in Various Areas[J];Spectroscopy and Spectral Analysis;2011-01
7 LIANG Qi-feng(Department of Chemistry,Jiaying University,Guangdong Meizhou 514015,China);Analysis of Honeys with Adding into Different Contents of Sucrose or Glucose by Infrared Spectrum[J];Guangzhou Chemical Industry;2010-01
8 Wang Weiwei,Ren Bengkang,Yan Ming,Shi Qiufang Institute of Life Science,Northwest University,Xian 710069;THE MUTATION BEEDING OF HIGH-YIELD GLA PRODUCING STRAIN RHIZOPUS ARRHIZUS USING He-Ne LASER[J];Acta Photonica Sinica;2002-02
9 ZHANG Hui,CUI Yan-peng,QIANG Xi-huai,SHU Jia-long(Resource and Environment Institute,Shaanxi University of Science and Technology,Xi'an,Shaanxi 710021,China);Graft modification of branched polyethylene wax with acrylic acid and emulsifying process[J];China Surfactant Detergent & Cosmetics;2013-01
10 Huang Xin;Chen Dongqing;Suzhou Diamond Metal Powder Co. Ltd;Longkou Environmental Protection Agency;;Study on Adsorption Properties for Uranyl Ion on Tea Scrap[J];Guangdong Chemical Industry;2013-22
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 LIANG Zhi-qi (College of Business of Beijing Union University,Beijing 100025,China);Application of Infrared Spectrum in Judgement of Counterfeits[J];JOURNAL OF BEIJING UNION UNIVERSITY;2000-02
2 Huang Hao, Li Jing, Qin Zhu, Zhou Qun, Sun Suqin* (Department of Chemistry, Tsinghua University, Beijing 100084);The Application of Fourier Transform Infrared Spectroscopy on the Quality Control of Traditional Chinese Medicine Formula Particles[J];Chinese Journal of Analytical Chemistry;2003-07
3 Cai Xilan (Experiment Center, Jiangsu Public Secu- rity College, Nanjing, 210012);Identification of mixed fibers by subtractive infrared spectroscopy[J];ANALYTICAL INSTRUMENTATION;2000-01
4 Shen WenhaoXie yiminLiu huanbin (State key Laboratory of Pulp & Paper Engineering, South China University of Technology, Guangzhou,510640);Application of Near_Infrared Spectroscopy in Pulp and Paper Industry[J];GUANGDONG PULP & PAPER;1999-02
5 Huang Weidong, Wang Junde, Che Xun and Song Guonan Dalian Institute of Chemical Physics, Academia Sinica, 116012 Dalian;ON-LINE NORMAL PHASE MICROBORE HPLC/FTIR METHOD[J];Spectroscopy and Spectral Analysis;1991-06
6 Dejuan LIN- a,b,Haibo PAN,Shuifa SHEN-a,Naisheng CHEN-a ,Jinling HUANG-a,Qiyu YANG-c and Hanhui ZHANG-c -aInstitute of Research on the Functional Materials,Fuzhou University,350 002 Fuzhou -bDepartment of Chemistry,Fujian Zhangzhou Teachers College,363000 Zhang zhou -cDepartment of Chemistry,Fuzhou University,350002 Fuzhou;FTIR Spectra of SO_4~(2-)/Fe_2O_3 Nanosolid Superacid[J];Spectroscopy and Spectral Analysis;2000-05
7 LIU Li-jun, JIANG Heng, GONG Hong, SU Ting-ting Liaoning University of Petroleum and Chemical Technology, Fushun 113001, China;The Improvement of Sample Preparation for Infrared Spectroscopy Analysis[J];Spectroscopy and Spectral Analysis;2004-01
8 WANG Duo-jia 1, 2, ZHOU Xiang-yang 1, JIN Tong-ming 1, HU Xiang-na 1, ZHONG Jiao-e 1, WU Qi-tang 2 1. Shenzhen Inspection Station of Non-pollution Agricultural Products, Shenzhen 518040, China 2. South China Agriculture University, Guangzhou 510000, China;Application of Near-Infrared Spectroscopy to Agriculture and Food Analysis[J];Spectroscopy and Spectral Analysis;2004-04
9 XU Liang 1, 2 , Suritalatu3, XI Hai-shan1, BI Kai-shun2, SUN Wurina1 1. Analysis and Testing Center of Inner Mongolia University for Nationalities, Tongliao 028042, China 2. School of Pharmacy, Shenyang Pharmaceutical University, Shenyang 110016, China 3. Affiliated Hospital of Inner Mongolia University for Nationalities, Tongliao 028042, China;Identification Study of Mongolian Herbal Medicine Rubus Sachalinesis Leveille and Its Forgeries by UV/Fluorescence/IR Spectroscopy[J];Spectroscopy and Spectral Analysis;2006-03
10 YANG Qun~1,WANG Yi-lin~1,YAO Jie~2,YU Hui-xiang~3 1.Department of Physics and Electronic Science,Chuxiong Normal University,Chuxiong 675000,China 2. Analyses and Testing Center,Nanjing Normal University,Nanjing 210097, China 3.The Institute of Yi Medicine,Province of Yunnan,Chuxiong 675000,China;A Rapid and Nondestructive Study of Yi Herbs Dahongpao and Jigen with Fourier Transform Infrared Spectroscopy[J];Spectroscopy and Spectral Analysis;2006-12
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved