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《Journal of Anhui Normal University(Natural Science)》 2006-03
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Preparation for Ferrocene Carboxylic Acid Modified Goldelectrode and Electrocatalytical Oxidation of Ascorbic Acid

XIE You-bin,LIU Hong-ying,DENG Xiang-hui,KAN Xian-wen,FANG Bin(College of Chemistry and Material Science,Anhui Normal University,Wuhu 241000,China)  
Ferrocene carboxylic acid /L-cysteine self-assembled gold electrode is prepared in this experiment.It is tokened by cyclic voltammetry and electrochemistry impedance.The electrochemical behavours of ferrocene carboxylic acid modified gold electrode are investgated in phosphorate buffer solution(pH=7.0),and the effect of medium and acidity on the cyclic voltammograms is investgated,too.The result obtained shows that the modified electrode exhibites a notable electrocatalytic response to the oxidation of ascorbic acid.The current is proportional to the concentration of ascorbic acid in the range of 2.52×10~(-5)-6.31×10~(-3) mol L~(-1).The detection limit is 1.30×10~(-6) and the correlative cofficient is 0.9931.
【Fund】: 安徽省自然科学基金(050460301)
【CateGory Index】: O657.1
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