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《Journal of Anhui Normal University(Natural Science)》 1994-03
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Study on Synthesis of 5 (4′ Hdo9eno 2′ Carboxy phenylazo) Rhodanine and Their Fluorescence.  ̄1H NMR. MS.

Wang Zhongyi; Shi Haijian; Shi Haoxin;Yang Zhoushen;Zheng Erhua(Department of Chemistry)(Test and Analysis Center)  
In this paper, we have synthesized three kinds of new organic fluorescencereagents: 4CRACP Ⅱ, 4B RACPⅢ. 4IRACP Ⅳ,Its structures were identifiedand fluorescence properties were studied. We find 4CRACP-Ⅱ has more intense fluo-rescence in the weak acid medium。 It reacts with copper(Ⅱ)at pH=5.3 to form fluo-rescenta coplex,λ_(ex)/λ_(em)=310nm/408nm. the detection limit was 0.5ng/g, we discussedthe influence of halogen on  ̄1H-NMR. MS.F.
【Fund】: 国家自然科学基金
【CateGory Index】: O62
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【References】
Chinese Journal Full-text Database 1 Hits
1 LI Man-xiu~*,DAI Yan-yun (Department of Chemistry,Xinzhou Teachers University,Xinzhou 034000,China);Development in research of artificial synthesized fluorescent reagents[J];化学试剂;2005-09
【Citations】
Chinese Journal Full-text Database 1 Hits
1 Liu Zhi-jie, Zhang Jian-heng, Jiang Lin (Department of Chemistry, Northwestern University, Xi' an, 710067);The Synthesis of 1-Phenyl-3-(3 '-Indolyl)-5-Substituted Phenyl-2-Pyrazolines and Their Substituent Effects in 1H NMR, MS[J];高等学校化学学报;1991-01
【Co-citations】
Chinese Journal Full-text Database 4 Hits
1 Wang,Meiyan Qu,Zhiqiang Du,Dan Jiang,Lin*(College of Chemistry and Material Science,Shandong Agricultural University,Taian 271018);Synthesis and Antifungal Activity of Novel 1-(3-Indoly)3-aryl-2-propen-1-one Oxime Ethers[J];有机化学;2013-05
2 LIN Zhi-ping,QIAO Feng-xia(Department of Biology and Chemistry,Baoding University,Baoding 071000,China);Progress in synthesis of 2-pyrazoline derivatives[J];河北大学学报(自然科学版);2012-03
3 Wang Zhongyi; Shi Haijian; Shi Haoxin;Yang Zhoushen;Zheng Erhua(Department of Chemistry)(Test and Analysis Center);Study on Synthesis of 5 (4′ Hdo9eno 2′ Carboxy phenylazo) Rhodanine and Their Fluorescence.  ̄1H NMR. MS.[J];安徽师大学报(哲学社会科学版);1994-03
4 Liu Zhi-jie, Jiang Lin, Zhang Jian-heng, Gong Yong (Department of Chemistry, Northwest University, Xi' an, 710069);The Synthesis of Indolyl-10H-Pyrido[1,2-a] Indolium Perchlorates[J];高等学校化学学报;1991-11
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 MING Yong_fei,XIE Yi,SUN Yu_xi,SHI Yun_wei,YOU Jin_mao (College of Chemistry, Qufu Normal Univesity,273165, Qufu,Sha ngdong,PRC);SEPARATION OF OLIGOPEPTIDES BY CAPILLARY ELECTR OPHORES IS USING 9-(2-CARBAZOLE)ETHYL CHLOROFORMATE(CEOC) AS DERIVATIZATION AGENT[J];曲阜师范大学学报(自然科学版);2003-04
2 GUO Qi-hua , LI Ying ,ZOU Hong,GU Xue-xin (Department of Chemistry, Capital Normal University, Beijing 100037), Huaxue Shiji,2003,25(5) ,288-290;A new labeling of fluorescent reagent for phenol——8-(4, 6-dichloro-1 ,3,5-triazinoxy) qoinaldine[J];化学试剂;2003-05
3 GE Xiao-xia, LIU Jin-kai, JIANG Chong-qiu" (Department of Chemistry, Shandong Normal University, Jinan 250014), Huaxue Shiji, 2003,25(5), 279-281;Synthesis and studies on fluorimetric quenching reaction be- tween beryllium and a new spectrofluorimetric reagent 2-hy- droxy-1-naphthaldehydene-hydrazinecarbothioamide[J];化学试剂;2003-05
4 MING Yongfei , SUN Yuxi, YOU Jinmao (Department of Chemistry, Qufu Normal University , Qufu 273165, Shandong, China);Separation of Amino Acids by Capillary Zone Electrophoresis Using 9-(2-Carbazole) Ethyl Chloroformate as Derivatization Agent[J];化学研究;2003-03
5 Yang Changxin , Xiao Xiangxu, Yangzhibin ( Jiangzhong Pharmaceutical Co. , Ltd. Jiangxi, Nancheng 330077 ; Department of Chemistry Nanchang University, Nanchang 330047), Huaxue Shiji,2003,25(1),20-22;Synthesis of 2,3-dihydroxyl quinoxaline and its applica- tion in the determination of trace lead[J];化学试剂;2003-01
6 HE Fang and JIANG Chong qiu* (Department of Chemistry, Shandong Normal University, Jinan 250014);Synthesis and studies on fluorimetric quenching reaction between beryllium and spectrofluorimetric reagent salicylaldehyde-hydrazinecarbothioamide[J];分析试验室;2002-06
7 ZHANG Ming-cui, SHANG Yong-jia, ZHU Yin-gui, WANG Lun (College of Chemistry and Materials Science , Anhui Normal University,Wuhu 241000, China);SYNTHESIS AND FLUORESCENCE PROPERTY OF A NEW FLUORESCENT REAGENT 5-(4-CHLOROPHENYLAZO)-8- SALICYLIDENEAMINOQUINOLINE[J];安徽师范大学学报(自然科学版);2001-04
8 Feng Suling *, Tang Anna, Fan Jing (College of Chemistry and Environmental Science,Key Laboratory of Environmental Science and Engineering, Education Commission of Henan,Henan Normal University,Xinxiang 453002);A Fluorescence Quenching Method for Determination of ArsenicⅢ[J];分析化学;2001-11
9 LONG Li ping,ZHENG Tong shen,LEI Cun xi (Department of Chemistry, Yiyang Teachers College, Yiyang, Hunan, 413049)$$$$;The Determination of β-Cyclodextrin by the Spectrophotofluorimetry[J];益阳师专学报;2001-03
10 ZHU Yan wu, ZHOU Yun you (College of Chemistry and Material Science, Anhui Normal University, Wuhu, Anhui, 241000, China);SYNTHESIS BY MICROWAVE AND FLUORESCENT PROPERTY OF 9-METHYLAGRIDINE[J];安徽师范大学学报(自然科学版);2001-02
【Secondary References】
Chinese Journal Full-text Database 1 Hits
1 LI Jian-ping~*,ZHENG Peng-zhi,ZHU Jun-ge,LIU Rui-jie,Qu Gui-rong (College of Chemistry and Environmental Science,Henan Normal University,Xinxiang 453007,China);An expedient method for the synthesis of bis(adipylhydrazones) under microwave irradiation in a solvent-free medium[J];化学试剂;2007-01
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