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《Anhui Medical and Pharmaceutical Journal》 2006-03
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Determination of loganin in liuwei dihuang oral liquid by HPLC

PAN Jian-de (Huangshan Tianmu Pharmaceutical Ltd.,Huangshan City,Anhui province,China 245000)  
Aim To determine loganin in liuwei dihuang oral liquid by HPLC.Methods Octadecylsilane chemically bonded silica was used as filling material.The mobile phase is tetra hydrofuran-methyl lyanide-carbinol-0.05% phosphoric acid solution(1∶8∶4∶87);The detection wavelength is at 236 nm.The temperature of detection wavelength column is 40℃.The theoretical plates is not lower than 4000 as calculated according to loganin area.The keeping time of loganin is 17~18 minutes.The quantity of inputting samples is 10 μl.Results The linear range is from 5~26 mg·L~(-1) for loganin,Y=20878.05X-224.51,r=0.9999.The average recovery of loganin for the added samples is at 95%~100%.Conclusion This experiment shows that this method is convenient,quick,exact,sensitive and reproductive.
【CateGory Index】: R286.0
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4 Bao En-quan1,Chen Ye-cang2(1.Chaohu Institute for Drug Control;2.Shanghai Haihong Group Chaohu C-dragon Pharmacy Co.,Ltd.Chaohu 238000);Determination of coganin in yunkang syrup by HPLC[J];Anhui Medical and Pharmaceutical Journal;2009-05
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6 SUN Guo-xiang,YANG Ting-ting(College of Pharmacy,Shenyang Pharmaceutical University,Shenyang 110016);Evaluation of the entire quality of Liuweidihuang pills by systematic quantified fingerprint based on chromatographic fingerprint resolution information index[J];Central South Pharmacy;2010-02
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9 HAN Duohong, MENG Hongmei(Department of Biology,Hexi College,Zhangye,Gansu 734000,China);Studies on tissue culture of Corydalis adunca and contents of alkaloid[J];Acta Botanica Boreali-occidentalia Sinica;2003-09
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5 ZHOU Jia-cai,LIANG Yu-mei(Nanjing Medical Hefei Tianxing Co.Ltd.,Hefei 230061);Determination of loganin in zhibodihuang capsules by HPLC[J];Anhui Medical and Pharmaceutical Journal;2008-11
6 DU Xiao-ying,SONG Yuan-zhi,ZHANG Ling,JIANG Jin-hua(Shaanxi Fangzhou Pharmaceutical Co.Ltd.Shaanxi Xi′an 710075,China);Quantitative Determination of Shidining in Bitongning Capsules by HPLC[J];Journal of Anhui Traditional Chinese Medical College;2005-06
7 HAN Ling-ling,HU Rong-feng,SUN Yu-liang(Anhui College of Traditional Chinese Medicine,Anhui Hefei 230038,China);Determination of Loganin of Qiju Dihuang Capsule by HPLC[J];Journal of Anhui Traditional Chinese Medical College;2007-02
8 WANG Wei~1,LIU Ning-yu~1,LI Jian-jun~2 (1.Henan Topfond Pharmaceutical Co.,Ltd.,Zumadian 463003,China;2.Department of Chemistry,Zhengzhou University,Zhengzhou 450052,China);Optimization of Condition for Extracting from Poria Cocos Wolf[J];Journal of Anyang Teachers College;2005-05
9 LI Ping WANG Yan-hui MA Run-yu (The Key Laboratory of Science and Technology of Controllable Chemical Reactions, Ministry of Education, Beijing University of Chemical Technology, Beijing 100029, China);Water extraction conditions of polysaccharide from Fructus Corni[J];Journal of Beijing University of Chemical Technology;2003-01
10 MA Jie, L Yue gang, HE Ya ming (College of Chemical Engineering, Beijing Technology and Business University, Beijing 100037,China);STUDY ON INFLUENCING FACTORS FOR TREATMENT OF SOYBEAN WASTEWATER USING PHOTOSYNTHETIC BACTERIA[J];Journal of Beijing Institute of Light Indusry;2000-01
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 Bao En-quan1,Chen Ye-cang2(1.Chaohu Institute for Drug Control;2.Shanghai Haihong Group Chaohu C-dragon Pharmacy Co.,Ltd.Chaohu 238000);Determination of coganin in yunkang syrup by HPLC[J];Anhui Medical and Pharmaceutical Journal;2009-05
2 HU Hong-ping1,YAN De-li2,ZHOU Wen-yan2(1.The People's Hospital of Shexian County,Shexian 245200,China;2.Traditional Chinese Medicine Rheumatism Hospital of Linquan,Linquan 236400,China);Determination of strychnine in renmatongbi pill by HPLC[J];Anhui Medical and Pharmaceutical Journal;2009-06
3 YANG Li-bin,LIU Shao-jing,BIAN Jun-chang,WEI Cai-xia,ZHANG Yun-peng(Xi'an Medical College,Xi'an,Shanxi 710021,China);Fat-soluble components in Cornus officinalis sieb.et Zucc[J];Anhui Medical and Pharmaceutical Journal;2010-11
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5 WANG Xiangjun1,CHEN Wen2*,ZHAO Yang3,WAN Zhenglan1,SONG Shuli1, DU Yu1,TANG Mingkun4,ZHAO Chenghua2(1.Biological Science and Technology College,Qiongzhou University,Provincial Key Laboratory of Amphibious and Reptile Research,Wuzhishan,Hainan 572200;2.Technical College,Qiongzhou University,Sanya,Hainan 572000;3.Environmental Protection Monitoring Center in Xinxiang,Xinxiang,Henan 453002;4.Sichuan Academy of Forestry,Chengdu,Sichuan 610081,China);Effects of Different Analytical Methods on Metal Pollution Index in Water[J];Guizhou Agricultural Sciences;2013-03
6 Yu Fang-rong,Li Xi-hai,Cai Liang-liang,Li Hui-ting, Chen Jia-shou,Weng Xia-ping,Ye Hong-zhi, Liu Xian-xiang;Study on the Effects of Different Polar Fractions of Tiaogu Tablet on the Activity of Chondrocytes[J];Rheumatism and Arthritis;2013-01
7 CAO Gui-xia1,WANG Xiu-yue2,JIAO Kun2(1.Fuyang Fourth People's Hospital,Fuyang,Anhui 236000;2.Fufang Institute for Food and Drug,Fuyang,Anhui 236015,China);Determination of loganin in Radix Dipsaci decocting pieces by HPLC[J];Anhui Medical and Pharmaceutical Journal;2013-05
8 YANG Ran1,CHAO Ya-nan1,LI Jian-jun1,QU Ling-bo1,2*(1.Department of Chemistry,Zhengzhou University,Zhengzhou 450052,China;2.Henan University of Industry,Zhengzhou 450001,China);Determination of Arsenic in Traditional Chinese Medicines Honeysuckle and Panpax Notoginseng by Chronopotentiometric Stripping Analysis[J];Physical Testing and Chemical Analysis(Part B:Chemical Analysis);2010-07
9 MO Luli,HUANG Hongfang,LIU Jiaju,et al.Department of Traditional Chinese Medicine,Dongsheng Hospital of Guangzhou in Guangdong Province,Guangdong,Guangzhou 510120;Observation of kidney-nourishing therapy of acupuncture combined with Traditional Chinese medicine therapy on osteoarthritis of knee joint[J];Hebei Journal of Traditional Chinese Medicine;2013-04
10 XU Yue,HU Ben-quan,WANG Yu(College of Pharmacy,Xi'an Medical University,Xi'an 710021,China);Determination of loganin in YinZi rehmannia glutinosa by RP-HPLC[J];Applied Chemical Industry;2012-09
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