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《Anhui Medical and Pharmaceutical Journal》 2015-11
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Quality standard study of the volatile oil of Qingre Jieji granules

LIU Xue;CUI Ying;HUANG Shun-wang;Anhui University of Traditional Chinese Medicine;Anhui Institute of Food and Drug Control,Anhui Provincial Key Laboratory of R&D of Chinese Medicine;  
Objective To establish quality standard of constituents of volatile oil from Qingre Jieji granules. Methods The TLC method was established to identify volatile oil of Qingre Jieji granules. The constituents of the volatile oil extracts were identified by GCMS. The content of volatile oil was determined by GC. Results The TLC spots were clear,reproducible,and the negative control showed no interference. GC-MS detected 13 chromatographic peaks and identified 12 compounds. The linear ranges of α-pinene,β-pinene and eucalyptol were 1. 89 ~ 605. 00 mg·L- 1( r = 1. 000),1. 25 ~ 99. 60 mg·L- 1( r = 1. 000),2. 32 ~ 185. 81 mg·L1( r = 1.000),respectively. The average recovery rates respectively were 92. 82%( RSD = 4. 83%),94. 29%( RSD = 3. 10%) and 104.23%( RSD = 3. 14%)( n = 9). Conclusions The method is reliable,accurate and specific,and it can be used for quality control of this preparation.
【CateGory Index】: R286.0;O657
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