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《Anhui Medical and Pharmaceutical Journal》 2015-11
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Quality standard study of the volatile oil of Qingre Jieji granules

LIU Xue;CUI Ying;HUANG Shun-wang;Anhui University of Traditional Chinese Medicine;Anhui Institute of Food and Drug Control,Anhui Provincial Key Laboratory of R&D of Chinese Medicine;  
Objective To establish quality standard of constituents of volatile oil from Qingre Jieji granules. Methods The TLC method was established to identify volatile oil of Qingre Jieji granules. The constituents of the volatile oil extracts were identified by GCMS. The content of volatile oil was determined by GC. Results The TLC spots were clear,reproducible,and the negative control showed no interference. GC-MS detected 13 chromatographic peaks and identified 12 compounds. The linear ranges of α-pinene,β-pinene and eucalyptol were 1. 89 ~ 605. 00 mg·L- 1( r = 1. 000),1. 25 ~ 99. 60 mg·L- 1( r = 1. 000),2. 32 ~ 185. 81 mg·L1( r = 1.000),respectively. The average recovery rates respectively were 92. 82%( RSD = 4. 83%),94. 29%( RSD = 3. 10%) and 104.23%( RSD = 3. 14%)( n = 9). Conclusions The method is reliable,accurate and specific,and it can be used for quality control of this preparation.
【CateGory Index】: R286.0;O657
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【Citations】
Chinese Journal Full-text Database 2 Hits
1 MA Wen-fang et al(Department of Pharmacy,Guangxi University of Chinese Medicine,Nanning,Guangxi 530001);Determination of α-pinene,Eucalyptol and Borneol in Volatile Oil from Zingiber officinale Roscoe by GC-MS[J];Journal of Anhui Agricultural Sciences;2012-21
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【Co-citations】
Chinese Journal Full-text Database 4 Hits
1 WANG Xi;CHEN You-sheng;College of Pharmaceutical Engineering,Guangdong Food and Drug Vocational College;;Determination of eucalyptol and α pinene in ointment[J];Anhui Medical and Pharmaceutical Journal;2014-07
2 Cui Chen;Geng Qi;Li Jingwei;Li Xin;Yang Xiaofan;Zhou Dan;Jiang Jian;Shuguang Hospital Affiliated to Shanghai University of Traditional Chinese Medicine;Yueyang Hospital Affiliated to Shanghai University of Traditional Chinese Medicine;;Analysis on Professor Jiang Jian's Experience of Releasing Migraine with Jiu Po Decoction[J];World Chinese Medicine;2015-07
3 PENG Zheng-Guo1,2,XUE Jian1,WU Xiao-bo1,XUE Wen1(1.Institute of Medicinal Plant Development,Chinese Academy of Medical Sciences,Peking Union Medical College,Beijing 100193,China;2.College of Pharmacy,Jiangxi University of Traditional Chinese Medicine,Nanchang 330004,China);Extraction and Stability Test of α-terpineol[J];Herald of Medicine;2011-09
4 YAO Yi-qian;ZHOU Li-ting;ZHU Hong-wei;ZHAO Hui-ming;School of Biological and Chemical Engineering,Jiaxing University;;Comparing Study of Ginger Oil Extraction from Xinfeng Ginger between Soxhelt Method and Steam Distillation Method[J];Journal of Jiaxing University;2013-06
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1 HU Rong LI Zulun YANG Lu∥Chengdu University of Traditional Chinese Medicine(Chengdu Sichuan 610075,China);Study on the Analgesic Effect of Imperatorin from Radix Angelicae Dahurica[J];Journal of Sichuan of Traditional Chinese Medicine;2012-04
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