Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Journal of Anhui Traditional Chinese Medical College》 2012-03
Add to Favorite Get Latest Update

Determination of 4,8-Dihydroxy-1-tetralone in the Hull of Carya Cathayensis Sarg by High Performance Liquid Chromatography

OU Jin-mei,CHEN Shi-yun,WU De-ling(School of Pharmacy,Anhui College of Traditional Chinese Medicine & Anhui Key Laboratory for Research and Development of Chinese Medicine,Anhui Hefei 230031,China)  
Objective To establish a high performance liquid chromatography(HPLC) method for determining the contents of 4,8-Dihydroxy-1-tetralone in the hull of Carya cathayensis Sarg.Methods The HPLC determination was carried out on a Shim-pack C18(250 mm ×416 mm,5 μm) column with mobile phase of methanol-water(40∶60),flow rate of 0.8 ml/min,column temperature of 25 ℃,and detection wavelength of 333 nm.Results The concentration of 4,8-dihydroxy-1-tetralone had a good linear relationship with the peak area within the range from 1.13 to 20.34 μg/ml(r=0.999 9).The average recovery was 101.8%,and relative standard deviation was 1.21%(n=6).Conclusion The established HPLC method can be used for determining the contents of 4,8-dihydroxy-1-tetralone in the hull of Carya cathayensis Sarg because of its accuracy,reliability,stability,and good reproducibility.
【CateGory Index】: R284.1;O657.72
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 6 Hits
1 SHEN Bing-xiang1,WU De-ling2,3,CHEN Shi-yun2,JIN Chuan-shan2,3,PENG Dai-yin2,3(1.The People′s Hospital of Lu′an,City,Luan Anhui 237005;2.Department of Pharmacy,Anhui College of Traditional Chinese Medicine,Hefei,Anhui 230031;3.Anhui Key Laboratory of Traditional Chinese Medicine,Hefei,Anhui 230031);Determination of total saponins in the Hull of carya cathayensis sarg[J];Anhui Medical and Pharmaceutical Journal;2009-05
2 CHEN Shi-yun,WU De-ling,JIN Chuan-shan,PENG Dai-yin,ZHAN Quan-sheng(1.Department of Pharmacy,Anhui College of Traditional Chinese Medicine & Anhui Key Laboratory of Traditional Chinese Medicine,Anhui Hefei 230031,China;2.Ningguo Zhanshi Natural Food Corporation Ltd.,Anhui Ningguo 242300,China);Preliminary Analysis on Chemical Components and Content Determination of Total Flavones in the Hull of Carya Cathayensis Sarg[J];Journal of Anhui Traditional Chinese Medical College;2010-01
3 Sun Guangren,Yao Dadi,You Shijiang(School of Forestry,Beihua University,Jilin 132013,P.R.China);Inhibition Effect of Green Walnut Peel on Several Human Pathogenic Bacteria[J];Journal of Northeast Forestry University;2009-01
4 YAO Huanying1, TANG Jingcheng2, ZHANG Anling2*, XU Yaoping2(1 Department of Chemistry, Weinan Normal College, Weinan,Shaanxi 714000 China; 2 College of Forestry, Northwest SciTech University of Agriculture and Forestry, Yangling Shaanxi 712100,China);Advances in research of the chemistry and bioactivity of Juglans plants[J];Acta Botanica Boreali-occidentalia Sinica;2003-09
5 ZHANG Ting,ZHANG Hong(College of Food Science and Engineering,Zhejiang Gongshang University,Hangzhou 310035);Research progress on chemical compounds of the green peel of carya cathayensis Sarg.and its biological activity[J];Food Science and Technology;2007-05
6 WU De-lin1,2,CHEN Shi-yun1,LIU Jing-song1,2,JIN Chuan-shan1,2,XU Feng-qing1,2 (1.College of Pharmaceutical Sciences of Anhui University of Traditional Chinese Medicine,Hefei 230031,China;2.Anhui Key Lab of Contemporary Traditional Chinese Medicine,Hefei 230031,China);Chemical Constituents of Carya cathayensis and Their Antitumor Bioactivity[J];Journal of Chinese Medicinal Materials;2011-07
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 TANG Li-chang et al(College of Horticulture and Landscape Architecture,Hainan University,Haikou,Hainan 570228);Analysis of the Volatile Component of the Invasive Plant-Eupatorium catarium Veldkamp[J];Journal of Anhui Agricultural Sciences;2011-10
2 LOU Fang-ming,LI Qun-fang,ZHANG Qian-ru,QIAN Jing (Zunyi Medical College,Guizhou 563003,China);Analysis of the essential oil from Helleborus thibetanus Franch. with GC-MS[J];Anhui Medical and Pharmaceutical Journal;2010-03
3 WANG Bin,CHEN De-huai,HUANG Dai,ZHU Jia-ru,ZHANG Xiao-xiang(Department of Pharmaceutical Engineering,Hefei University of Technology,Hefei 230009,China);Extraction,separation and acute toxicity test of saponins in Momordica cochichinensis[J];Anhui Medical and Pharmaceutical Journal;2011-02
4 LIU Ya-min~1, XU Yao-ping~1, GAO Jin-ming~(2*), YANG Xiou-ping~1, LIU Yu-sheng~1 (1 College of Forestry, Northwest Sci-Tech University of Agriculture and Forestry, Yangling,Shaanxi 712100, China;2 National Engineering Research Center for Phytochemistry in West China, Yangling ,Shaanxi 712100,China);Analysis of volatile components from leaves of Juglans regia By GC/MS[J];Acta Botanica Boreali-occidentalia Sinica;2004-06
5 ZHAI Mei-zhi,YAN Ting,WANG Yuan,JIA Cai-xia(College of Forestry,Northwest A&F University,Yangling,Shaanxi 712100,China);Research Advances on Chemical Ingredients and Biological Activity of Green Husk and Leaves from Juglans L.[J];Acta Botanica Boreali-Occidentalia Sinica;2011-10
6 YAN Fang ( Rural Energy Office of Linan,Linan,Zhejiang 311300);Advance in Resource Utilization of Agricultural and Forestry Waste Hickorg Epicarp[J];Journal of Anhui Agricultural Sciences;2013-14
7 WANG Jing,Lü Fang-de(Nonwood Forest Research Institute,Central South University of Forestry & Technology,Changsha 410004,Hunan,China);Advances in research on Carya Nutt in China[J];Nonwood Forest Research;2012-01
8 KANG Wen-yi1,2,SONG Yan-li1,2,LI Cai-fang1,2(1.Institute of Natural Products,Henan University,Kaifeng 475004,Henan,China;2.Pharmaceutical College of Henan University,Kaifeng 475004,Henan,China);Antioxidant Activity of Juglans Regia L.[J];Fine Chemicals;2009-03
9 CHEN Hang-jun1 LI Xing-fei 1,2 GAO Hai-yan 1 FANG Xiang-jun 1(1.Food Science Institute,Zhejiang Academy of Agricultural Science,Hangzhou,Zhejiang 310021; 2 College of Chemistry and Life Sciences,Zhejiang Normal University,Jinhua,Zhejiang 321004);THE ANALYSIS OF CHEMICAL COMPOSITION AND ANTIOXIDANT ACTIVITIES OF PHENOLIC COMPOUNDS FROM CARYA(CARYA CATHAYENSIS) KERNEL[J];Journal of Nuclear Agricultural Sciences;2013-01
10 YANG Hua,MA Rong-xuan,SONG Yan-wei(College of Chemistry and Chemical Engineering,Yan’an University,Yan’an 716000,China);Study on Inhibitive Activity of Walnut Peel’s Extracts on Seedling Growth of Some Crops[J];Acta Agriculturae Jiangxi;2013-05
China Proceedings of conference Full-text Database 1 Hits
1 WU Xiao-jun,WU Wei,ZHAO Yu-qing(School of Traditional Chinese Materia Medica,Shenyang Pharmaceutical University,Shenyang 110016,China);Advances in studies on modern pharmacy of Carya cathayensis[A];[C];2011
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 ZHAO Zhi-gang(Historical Culture College,Beihua University,Jilin,Jilin 132013);Analysis and Evaluation on Fatty Acid Composition of Hickory Nut Oil[J];Journal of Anhui Agricultural Sciences;2009-06
2 WEI Xiu-lai1,GAO Chang-kun1,GAO Jian1,XU Xian-xiang2(1.Dept of Pharmacy,The First Affiliated Hospital of Anhui Medical University,Hefei Anhui 230022;2.Dept of Pharmacy,The First Affiliated Hospital of Anhui College of TCM,Hefei Anhui 230038);Determination of total saponins in achyranthes bidentata[J];Anhui Medical and Pharmaceutical Journal;2007-05
3 ZHANG Ting-ting,LI Jing,WANG Cheng-yong(School of Pharmacy,Anhui College of Traditional Chinese Medicine,Anhui Key Laboratory of Modernized Chinese Material Medical,Hefei 230038,China);Extraction technology for the total saponin of Chaenomeles speciosa[J];Anhui Medical and Pharmaceutical Journal;2009-02
4 SHEN Bing-xiang1,WU De-ling2,3,CHEN Shi-yun2,JIN Chuan-shan2,3,PENG Dai-yin2,3(1.The People′s Hospital of Lu′an,City,Luan Anhui 237005;2.Department of Pharmacy,Anhui College of Traditional Chinese Medicine,Hefei,Anhui 230031;3.Anhui Key Laboratory of Traditional Chinese Medicine,Hefei,Anhui 230031);Determination of total saponins in the Hull of carya cathayensis sarg[J];Anhui Medical and Pharmaceutical Journal;2009-05
5 WU De-ling,JIN Chuan-shan,LIU Jin-qi,SHAO Hai-feng(Department of Pharmacy,Anhui College of Traditional Chinese Medicine,Anhui Hefei 230031,China);Quantitative Determination of the Total Flavanone Content in Fructus Alpinia Oxyphylla[J];Journal of Anhui Traditional Chinese Medical College;2005-06
6 CHEN Shi-yun,WU De-ling,JIN Chuan-shan,PENG Dai-yin,ZHAN Quan-sheng(1.Department of Pharmacy,Anhui College of Traditional Chinese Medicine & Anhui Key Laboratory of Traditional Chinese Medicine,Anhui Hefei 230031,China;2.Ningguo Zhanshi Natural Food Corporation Ltd.,Anhui Ningguo 242300,China);Preliminary Analysis on Chemical Components and Content Determination of Total Flavones in the Hull of Carya Cathayensis Sarg[J];Journal of Anhui Traditional Chinese Medical College;2010-01
7 LAN Ying1,FANG Jinbo1,ZHANG Weijing2,CHANG Yaping3(1Institute of Genetics and Cytology,Northeast Normal University,Changchun 130024,China;2Northeast Normal University Hospital, Changchun 130024,China;3Basic School of Medical Sciences,Jilin University,Changchun 130021,China);The experimental study on mice tumor necrosis factor production of GPJM (aqueous extract)[J];Journal of Northeast Normal University (Natural Science Edition);2003-01
8 LIU Ya-min~1, XU Yao-ping~1, GAO Jin-ming~(2*), YANG Xiou-ping~1, LIU Yu-sheng~1 (1 College of Forestry, Northwest Sci-Tech University of Agriculture and Forestry, Yangling,Shaanxi 712100, China;2 National Engineering Research Center for Phytochemistry in West China, Yangling ,Shaanxi 712100,China);Analysis of volatile components from leaves of Juglans regia By GC/MS[J];Acta Botanica Boreali-occidentalia Sinica;2004-06
9 Wang Shuping 1,2, Meng Xiangying *1, Qi Xiaoli 1, Zhang Xiaolu 1, Bo Huaben 1, Wu Yin 1, Bao Yongli 1, Li Yuxin *1 1 (Institute of Genetic and Cytology , Northeast Normal University , Changchun 130024) 2(Department of Applied Chemistry, Changchun Institute of Technology, Changchun 130022);Analysis of the Volatile Oil from the Stem-Bark of Juglans Mandshurica Maxim(L.)[J];Chinese Journal of Analytical Chemistry;2005-07
10 CHEN Xiang-ming1,2,YU Zhi-min2,JIN Jie2 and LIU Mei-xia3(1.Agronomy College,Gansu Agricultural University,Lanzhou 730072;2.Department of Biological and Environmental Engineering,Hefei College,Hefei 230022;3.Department of Chemical Engineering,Anhui science and teachnology University,Huainan 232001),Fenxi Shiyanshi,2007,26(8): 45~47;Studies on the inorganic composition of Hickory Hull[J];Chinese Journal of Analysis Laboratory;2007-08
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved