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Determination of Gibberellin Residues in Fruits and Vegetables by Liquid Chromatograpy-Tandem Quadrupole Mass Spectrometry

LIU Yan-qin WANG Hao YANG Hong-mei GUO Qi-lei SHI Hai-liang YAN Long-bao(National Food Quality and Safety Supervision and Inspection Center,Beijing 100094)  
This study developped a LC/MS/MS method for the determination of gibberellin residues in fruits and vegetables.Samples were extracted with 50% acetonitrile water solution(pH 2.50),then seperated in ZORBAX SB-Aq column(2.1mm×150.0mm,3.5μm)with mobile phase of methanol and 0.1% formic acid(40∶60 by volume).The mass spectrometry was operated in the positive ion mode of multiple reaction monitoring.The limit of detection was 2.0 μg/L,and the quantitative lower limit was 10 was in fruits and vegetables.The linear range was between 2.0μg/L and 10.0μg/L.The recovery rate was between 90.1% and 102.3%,and the relative stantard deviation was 4.07%.
【CateGory Index】: S481.8
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