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《Journal of Anqing Teachers College(Natural Science Edition)》 2002-04
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Beckmann Rearrangement of Benzophenoneoxime under Ultrasonic Irradiation

ZHOU Hong,HUANG Wei(Department of Chemistry, Anqing Normal College , AnqingAnhui 246011,China)  
Ultrasound is used frequently in organic synthesis in recent three decades. Benzanlilide is an important dyepharmaceutical intermediate.Beckmann arrangement of benzophenoneoxime catalyzed by polyphosphoric acid under ultrasonic irradiation is studied, from which benzanlilide could be obtained. The temperature of this reaction is low, and the yield is 80~90%. Mechanism of the reaction under ultrasonic irradiation is also discussed.
【CateGory Index】: O621.3
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