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《Journal of Anqing Teachers College(Natural Science Edition)》 2003-01
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Molecular Based Magnets with Layer Structure {[ML][Fe(Ⅱ)Fe(Ⅲ)(ox)_3·1.5H_2O]}_∞:Syntheses,Spectra Characterization (M=Co~(2+) ,Mn~(2+) )

LIU Guang xiang,CHEN You cun (Chemistry Dept.of Anqing Teachers College,Anqing 246011,China)  
Two new Schiff base complexes,CoL(ClO 4)·3H 2O(1) and MnL(ClO 4)·3H 2O(2) {L are condensed from equation molar salicylaldehyde and diethylenetriamine}has been synthesized and characterized.Further more two new bimetallic coordination polymers,{[Fe ⅡFe Ⅲ(ox) 3]·1.5H 2O} ∞,are synthesized and characterized,where ox 2- =oxalate,M=Co 2+ (3)or Mn 2+ (4).The results of the IR and M o¨ssbauer spectra of(3) and (4) reveal that two bimetallic coordination polymers exist in 2 D layer structure in the solid state,and anions layer is formed by [Fe ⅡFe Ⅲ(ox) 3] - unit.
【Fund】: 安徽省教委自然科学基金资助(2001kj162)
【CateGory Index】: O641.4
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