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《Journal of University of Science and Technology Liaoning》 2009-03
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New technique on iodination of substituted anilines

DONG Yan,LEI Peng,HU Zhi-zhi(School of Chemical Engineering,University of Science and Technology Liaoning,Anshan 114051,China)  
Some aromatic iodo compounds were synthesized by using some substituted anilines as the raw materials via the iodination.The focus of the study was to optimize the synthesis methods,reaction temperature and reaction time for 2,4-dichloroaniline substrate.The optimum reaction conditions are as follows: by selecting iodine mono-chloride solution,reaction temperature is 70 ℃,reaction time is 4 h.Under this optimum condition,the yield reaches 65.2%.The structures of the target products are identified by IR,MS and NMR.
【Fund】: 辽宁省教育厅高等学校科学研究资助项目(2004064D064)
【CateGory Index】: O621.25
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