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《Chinese Journal of Semiconductors》 2005-02
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Effects of Polyethylene Glycol Concentration on Properties of Nanocrystalline Titania Porous Films

Bu Shaojing,Jin Zhengguo,Liu Xiaoxin,Yang Lirong,and Cheng Zhijie(Key Laboratory for Advanced Ceramics and Machining Technology of Ministry of Education, School of Materials,Tianjin University,Tianjin 300072,Chinese)  
Nanocrystalline titania porous films are prepared on glass substrates via a sol-gel dip-coating method from a tetrabutylorthotitanate solution that contains diethanolamine as the stabilizer of titanium alkoxide and polyethylene glycol (PEG) as a template.The pore size is tunable in range of 10~1000nm.The influence of PEG(1000) concentration upon the properties of the TiO 2 films is studied by means of ESEM,AFM,UV-VIS,viscosity measurement,N 2-adsorption,XPS,and XRD.Experimental results show that at the PEG amount of 4 0g in 100mL solution,a three-dimensionally extended porous structure can be obtained,in which fine-shaped pores sized from 200 to 500nm are distributed homogeneously.The surface area of the film is 76 1m2/g.Nevertheless,excessive addition of PEG leads to deterioration of the film properties.
【Fund】: 天津市重点基础研究资助项目 (批准号 :F10 3 0 0 4)~~
【CateGory Index】: O614.33
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