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《Chinese Journal of Explosives & Propellants》 2002-01
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Study on the Lab. Synthesis of HMX Using Dinitrogen Pentoxide as the Nitrating Agent

GE Zhong xue, LI Gao ming, HONG Feng, SONG Xin chao (Xi′an Modern Chemistry Research Institute, Xi′an 710065, China)  
The method of synthesizing HMX is presented in this paper. Using DADN(1,5 diacetyl 3,7-dinitro 1,3,5,7 tetranitrotetrazacycloctane) as reactant, the HMX was synthesized in the nitrating agent of the mixture of dinitrogen pentoxide and nitric acid. The yield of HMX was more than 96%, mp 272.0~272.8℃. In addation, factors that affecting the yield of HMX were discussed preliminely.
【CateGory Index】: TQ560
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【References】
Chinese Journal Full-text Database 4 Hits
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1 L U·· Zao sheng, L U·· Chun xu (Nanjing University of Science and Technology, Nanjing 210094, China);A Kind of New Green Nitration Technology[J];Chinese Journal of Explosives & Propellants;2000-04
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【Co-citations】
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1 Lü Zao-sheng~1, WANG Xiao-yan~1, Lü Chun-xu~2(1. Wuhan University of Science and Technology, Hubei430081, China; 2. Nanjing University of Science & Technology , Nanjing210094, China);Macro-kinetics Study of Ozone-mediated Nitration Reaction of Aromatic Compounds with Nitrogen Tetroxides[J];Chinese Journal of Explosives & Propellants;2004-03
2 XI Li-min~(1),KE Zhong-lu~(2)(1.Departement of Biological and Chemical Engineering,Taizhou Technical college,Taizhou 318000 China)(2.college of Materials and Chemical Engineering,Zhejiang university,Hangzhou 310027,China);Preparation of Nanosolid Superacid SO_4~(2-)/ZrO_(2)-Fe_(2)O_(3) and Study on Catalytic Synthesis of Nitrobenzene[J];Journal of Molecular Catalysis;2006-05
3 XI Li-min,YAN Qi-dong,JIANG Jun-rong(Departement of Biological and Chemical Engineering,Taizhou Vocational Technical College,Taizhou 318000,China);Nitrobenzene synthesis technology using Fe_2O_3/SO~(2-)_4 solid super acid as the catalyst[J];Industrial Catalysis;2006-02
4 Li Xiaoqing,Du Xiaohua,Zheng Mei,Chen Sheng,Xu Zhenyuan(Catalytic Hydrogenation Research Center,State Key Laboratory Breeding Base of Green Chemistry-Synthesis Technology,Zhejiang University of Technology,Hangzhou 310014);Research Progress of Green Nitration[J];Chemical Industry and Engineering Progress;2005-10
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6 ZHANG Qi rong,ZUO Jun,CHEN Xue lin,YU Wei fie (Institute of Chemical Material,China Academy of Engineering Physics,Mianyang 621900,China);Synthesis and application of nirto-pyridine derivatives[J];Chemical Research and Application;2002-04
7 XILi-min,YANQi-dong,JIANG Jun-rong(Department of Biological and Chemical Engineering,Taizhou Technical College,Taizhou 318000,China);Synthesis of aromatics nitration catalyzed by solid super acid ZrO_2/SO_4~(2-)[J];Shaanxi Chemical Industry;2005-10
8 CHENG Guang Bin *, LU·· Chun Xu, PENG Xin Hua(School of Chemical Engineering,Nanjing University of Science and Technology,Nanjing 210094);Regioselective Synthesis of Mononitrochlorobenzene (Ⅱ)Nitration with Nitrogen dioxide[J];Chinese Journal of Applied Chemistry;2002-02
【Co-references】
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1 Yan Qidong Xu Jun(Departement of Biological and Chemical Engineering ,Taizhou Vocational Technical college,Zhejiang Taizhou 318000,China);Research on MCM-41zeolite-catalyzed Benzene Nitration[J];Anhui Chemical Industry;2005-06
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4 L U·· Zao sheng, L U·· Chun xu (Nanjing University of Science and Technology, Nanjing 210094, China);Synthesis of Mononitrochlorobenzene by Green Nitration Technology[J];Chinese Journal of Explosives & Propellants;2000-04
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9 Cao Duan-lin, Cao Ming-bao, Li Yong-xiang (Dept.of Chemical Engineering, North China University of Technology, Taiyuan030051, China);Synthesis of Keto-RDX Using Dinitrogen Pentoxide as the Nitrating Agent[J];Chinese Journal of Explosives & Propellants;2004-01
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4 HAN Qi-long, WANG Xuan-jun, JIANG Da-yong ( The Second Artillery Engineering College, Xi,an 710025, China );Research Progress in Treatment Technology of Obsolete Solid Propellant[J];Chemical Propellants & Polymeric Materials;2008-06
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