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《Journal of Zhejiang University of Traditional Chinese Medicine》 2008-03
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HPLC Measure the Content of Emodin in Raw and Prepared Fleece-flower Root

Yang Xianling Red Cross Taiwang Compatriot Hospital of Xiangshan County,Zhejiang Province(315731)  
[Objective]Make measurement of emodin content in raw and prepared fleece-flower root.[Method]Take HPLC and the color-spectrum column SPHERISORB ODS2(150×4.6mm,5μm),the flow spectrum being methanol –0.1% phosphate(85:15),the measurement wave length:254nm,column temperature:28℃,flow speed:1.0 ml·in-1.[Result]The regression equation Y=3352.3X+37.297,the linear range:0.03~0.20μg,the average reception rate of the raw fleece-flower root:96.6%(RSD=1.3%).[Conclusion]The said method is correct and quick,with good repeat,can be used for quality control of fleece-flower root drug.
【CateGory Index】: R286
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Chinese Journal Full-text Database 3 Hits
1 Liu Sankang,Qian Guangsheng and Li Zhangwan (School of Pharmacy,West China University of Medical Sciences,Chengdu,610041);RP-HPLC Determination of Emodin in Radix Polygoni Multiflori Preparata and Four Kinds of Related Chinese Patent Medicines[J];Chinese Journal of Pharmaceutical Analysis;1998-06
2 Guo Qing (Jiangsu Provincial Institute of Drug Control,Nanjing 210008) Lu Jing (National Institute for the Control of Pharm.& Bio.Products,Beijing 100050);HPLC Determination of Anthraquinone in Radix Polygoni Multiflori and Radix Polygoni Multiflori Preparata[J];CHINESE JOURNAL OF PHARMACEUTICAL ANALYSIS;2000-05
3 LI Yi ping, ZHANG Sheng chun *, YANG Guang de (College of Pharmacy, Xi'an Jiaoton University Xi'an 710061, China);Study on the extraction methods of emodin from Radix polygoni multiflori[J];Chinese Traditional Patent Medicine;2004-04
Chinese Journal Full-text Database 10 Hits
1 SHI Ya-jun1,ZHANG Li2(1.Shanxi University of Traditional Chinese Medicine,Xianyang Shanxi,712046,China)2.Affiliated Hospital of Shanxi University of Traditional Chinese Medicine,Xianyang Shanxi 712000 China);Extraction technique of reducing blood lipids effective components from radix polygoni multiflori[J];Anhui Medical and Pharmaceutical Journal;2009-02
2 WU Ting~1,WANG Chao~2,LI Jie~1,LI Nan~1(1.College of Science,China Agricultural University,Beijing 100094,China;2.Chinese Academy of Inspection and Quarantine,Beijing 100025,China);Determination of anthraquinone-compound in cosmetics by high performance liquid chromatography[J];China Surfactant Detergent & Cosmetics;2006-01
3 DING Zhen,ZHANG De-zhi(Institue of Pharmacy,Guangdong College of Pharmacy,Guangzhou,Guangdong 510006,China);Preparation of emodin by demethylation[J];Journal of Guangdong College of Pharmacy;2007-01
4 YAN Han-Jing1,2,LIANG Lu-Jiao2,FANG Zhi-Jian2(1.College of Life Sciences,Zhongshan University,Guangzhou 510275,China;2.Guangdong Pharmaceutical University,Guangzhou 510006,China);Anatomical characteristics of leaf epidermis of Fallopia multiflora and relationships to climate factors[J];Guihaia;2009-01
5 TIAN Xiao dong YU Gui Xin PAN Hong bin (Department of pharmacy, Shenzhen nanshan peoples hospital, Shenzhen, 518051);Determination of total emodin in Huangqi liniments by RP-HPLC[J];Strait Pharmaceutical Journal;2001-02
6 WANG Hai-Ying1 LI Hong-Mei1 SHI Nan1 WEI Jiang-Chun1,2 (1The Life Science College of HeiBei University, Baoding 071002) (2The Institute of Microbiology, The Chinese Academy of Sciences, Beijing 100080);THE HPLC ANALYSIS OF THE LICHEN SUBSTANCES IN FIVE SPECIES OF XANTHORIA (ASCOMYCOTA)[J];Mycosystema;2003-04
7 Ting Wu1,Nan Li1,Jie Li1,Chao Wang2*(1. College of Science, China Agricultural University ,Beijing 100094; 2. Chinese Academy of Inspection and Quarantine, Beijing 100025 );The Recent Research of the Anthrquinones[J];Life Science Instruments;2005-05
8 LI Jing1,2,ZHANG Li2,CAO Ling2,WANG Yu2 (1.China Pharmaceutical University,Nanjing 210009,China;2.Jiangsu Institute for Food & Drug Control,Nanjing 210008,China);Determination of the content of Emodin in Shouwu Pills by HPLC[J];Chinese Journal of Biochemical Pharmaceutics;2009-02
9 XIE Hua1 MA Yue-ming1 ZHANG Ning2 1. College of Pharmacy, Shanghai University of Traditional Chinese Medicine; 2. Experimental Center of Science and Technology, Shanghai University of Traditional Chinese Medicine;Determination of Anthraquinones and Amygdalin in "Taohe Chengqi Decoction" by HPLC[J];Shanghai Journal of Traditional Chinese Medicine;2006-07
10 DUAN Yan-bing~1,HAN Yu-wan~2,JIN Jun~3,CHEN Wan-sheng~(4*)(1.Pharmacy School of The Second Military Medical University,Shanghai 200433,China;2.Official Hospital of Nangjing Military District,Nanjing,Jiangsu 210016,China;3.Yangtze Pharmaceutical Group,Nanjing,Jiangsu 210049,China;4.Changzheng Hospital Affiliated to the Second Military Medical University,Shanghai 200433,China);Determination of Emodin Content in Meibao Capsules[J];LiShiZhen Medicine and Materia Medica Research;2006-01
【Secondary Citations】
Chinese Journal Full-text Database 6 Hits
1 Zhang Yuhua 1,Zhang Jin 2 1. Wuhan Traditional Chinese Medicine Corporation.Wuhan 430064 2. Wuhan Mayinglong Pharmacg Corporation.Wuhan 430064;Determination of Content of the Emodin and Glycoside in Fleece-flower Root and Its Preparation by Thin-layercolorimetric Method[J];Jounal of Hubei College of Trditional Chinese Medicine;2000-04
2 Guo Qing (Jiangsu Provincial Institute of Drug Control,Nanjing 210008) Lu Jing (National Institute for the Control of Pharm.& Bio.Products,Beijing 100050);HPLC Determination of Anthraquinone in Radix Polygoni Multiflori and Radix Polygoni Multiflori Preparata[J];CHINESE JOURNAL OF PHARMACEUTICAL ANALYSIS;2000-05
3 Zhu Lianhua, Wang Zhihua (Technical Research Center of State Traditional Chinese Materia Medica Engineering, Shanghai, 200127);Quality Analysis of Radix Polygoni Multiflori from Different Areas[J];CHINESE TRADITIONAL PATENT MEDICINE;1999-01
4 Yuan Hailong, Zhang Chun, Li Xianyi, et al (Pharmaceutical College of the Second Military Medical University, Shanghai 200433);Determination of Rhein, Emodin and Physcion in Tuber Fleeceflower (Polygonum multiflorum) by Supercritical Fluid Extraction-HPLC[J];CHINESE TRADITIONAL AND HERBAL DRUGS;1999-04
5 College of Pharmacy, Beijing University of Medical Sciences (Beijing 100083) Yang Donghui, Cai Shaoqing and Wang Xuan College of Chinese Materia Medica, Beijing University of TCM and Chinese Materia Medica Wei Luxue;Determination of Emodin and Physcion in Capsules of Tuber Fleeceflower (Polygonum multiflorum) and Its Complex Prescription with Cordycep by HPLC[J];CHINESE TRADITIONAL AND HERBAL DRUGS;2000-03
6 Chen Dingyi. Wang Jingzhu and Zhao Xianhong(Beijing University of Traditional Chinese Medicine 100029);Analytical Study on processing of Rheum palmatum L. by HPLC[J];CHINA JOURNAL OF CHINESE MATERIA MEDICA;1994-09
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