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《Acta Armamentarii》 2005-06
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Influence of Anti-solvent Property on the Modes of Crystallization of HNIW

JIN Shao-hua,LEI Xiang-dong,OU Yu-xiang,LIU Jin-quan,SONG Quan-cai(School of Material Science and Engineering,Beijing Institute of Technology,Beijing 100081,China)  
A study on the methods and processes of crystallization of ε-HNIW was given,and a theoretical explanation of its crystal transformation was found in this paper.The solubility of HNIW almost does not change with variations in the temperature of solution.Therefore only the anti-solvents involved in crystallization is effective in the preparation of ε-HNIW.It is revealed that the physical properties such as the dipole moment and molecular polarity of the anti-solvent play an important role in the process of crystallization of HNIW.When using acetic ether or acetone as the solvents,anti-solvents with lower values of dipole moment,for example petroleum ether,isooctane,cyclohexane,toluene etc,make the HNIW to form an ε-modification,whereas anti-solvents with higher values of dipole moment,such as triethylene glycol,to form other modifications of HNIW.At higher temperatures,the duration that ε-HNIW can keep its modification is longer in non-polar solvents than in polar solvents.
【Fund】: 国防科技预研基金项目(00J12.6.6.BQ0127)
【CateGory Index】: TQ560.1;
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