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《Journal of Beijing University of Chemical Technology》 2004-03
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Preparation of NiO nanoparticles by homogeneous precipitation method and its characterization

Guo Guang sheng Zheng Dong hua Wang Zhi hua Lu Jie huan Guo Hong you(The Key Laboratory of Science and Technology of Controllable Chemical Reactions, Ministry of Education, Beijing University of Chemical Technology, Beijing 100029, China)  
NiO nanoparticles were prepared by a homogeneous precipitation method with an aqueous solution of nickel nitrate hexahydrate and urea. The effects of Ni(NO 3)2·6H 2O/CO(NH 2) 2 ratio, reaction temperature and heat treating temperature on NiO yield and mean size were discussed. The samples of NiO precursors and particles were characterized by TG DTA, XRD, TEM, etc. It was found that the decomposition temperature of the precursor began at 320?℃. The prepared NiO particles under optimum conditions are pure with a spherical shape and a mean size of 15?nm and well dispersed. The particles are of a single crystal phase (belong to cubic syngony).
【Fund】: 国家自然科学基金资助项目 (2 0 2 71 0 0 6 )
【CateGory Index】: O614
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