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《Journal of Beijing University of Chemical Technology》 2005-03
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Synthesis and property of core-shell microsphere with phase-transfering by infrared laser

FENG Yu-guang1 LI Zhong-xiao2 ZHANG Yu-chuan1 PU Jia-ling2 (1.College of Materials Science and Engineering,Beijing University of Chemical Technology, Beijing 100029; 2.The Major Laboratory of Printing and Packaging Engineering, Beijing Institute of Graphic Communication, Beijing 102600,China)  
A novel microsphere of an average diameter 55?nm was synthesized. The shell of the microsphere converted from hydrophilicity into hydrophobic nature by infrared laser. The core was synthesized mainly with methyl methylacrylate (MMA). The shell was synthesized with glycidyl methylacrylate (GMA) before it was modified by quarternary ammonium salt. The configuration of the micro-sphere was characterized by infrared spectrum (IR) and transparent electronic microscope (TEM); and its calorific property was characterized by differential scanning calorimeter (DSC) and thermogravimetric analysis (TG). The hydrophilic ability of the microsphere was tested by contact angle of water. The effects on the phase transformation were discussed. As a result, the glass transferring temperature (T_g) of the core is 56.2?℃ and the T_g of the shell is 85.3?℃. The value of the contact angle of water on the coating of core-shell microsphere was 20° and became 93° after radiation from infrared laser.
【Fund】: 北京市教委“科技发展计划”项目(00kj129)
【CateGory Index】: TB383
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