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《Journal of Beijing University of Chemical Technology(Natural Science Edition)》 2007-05
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Preparation of ultrafine silica with different morphologies using reverse microemulsions

SHEN ShuLing1 WU Wei2 GUO Kai1 CHEN JianFeng1,2 (1.Research Center of the Ministry of Education for High Gravity Engineering and Technology;2.Key Laboratory for Nanomaterials,Ministry of Education,Beijing University of Chemical Technology,Beijing 100029,China)  
Ultrafine silica particles with different morphologies have been prepared in water/toluene/sodium dodecylsulphate/1-pentanol water in oil microemulsion systems by means of penetration reactions and amalgamation reactions.The phase diagrams for the W/O microemulsion were plotted to study the relationship between the W/O microemulsion composition and the preparation conditions.The effects of varying the process and the value of R(ratio by mass of water:(surfactant +cosurfactant)) on the shape and size of the resulting silica particles were studied.A mechanism for the formation of ultrafine silica by the different reaction pathways has been proposed.
【Fund】: 国家自然科学基金重点项目(20236020);; 国家杰出青年基金(20325621)
【CateGory Index】: O613.72
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