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《JOURNAL OF BEIJING UNIVERSITY OF CHEMICAL TECHNOLOGY》 1997-03
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The Preparation and Characterization of Hydrotalcite and Hydrotalcite like Compounds

Du Yibo He Jing Li Feng D G Evans Duan Xue Wang Zuoxin (Departmint of Applied Chemistry,Beijing University of Chemical Technology,Beijing,100029)  
Hydrotalcite Mg 6Al 2(OH) 16 CO 3·4H 2O and the hydrotalcite like materials Mg 4Al 2(OH) 12 (NO 3) 2·4H 2 and Zn 6Al 2(OH) 16 CO 3·4H 2O have been prepared. X ray diffraction shows that their structures are similar,their interlayer spacings being 0 791nm、0 898[KG*1/4]nm and 0 773nm respectively. Their thermal stabilities are not high,all the crystal water being lost on heating to 200℃,and all the interlayer anions and most of the OH - ions in the layers being lost on heating to 500℃ . A pollared hydrotalcite like compound Mg 4Al 2(OH) 12 [C 10 H 6(SO 3) 2]·4H 2O has been prepared by both anion exchange and co precipitation methods. X ray diffraction shows that very similar materials are obtained in each case,their interlayer spacing varying between 1 577 and 1 544nm depending on method of preparation and drying conditions.
【Fund】: 国家自然科学基金
【CateGory Index】: O611.4
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1 WU Yan;LEI Yan-qing;LIU Xin-yue;QIU Yue;WANG Hao;School of Chemistry and Chemical Engineering,Southwest Petroleum University;;Synthesis and characterization of 12-tungstophosphoric acid intercalated MgAl layered double hydroxides and their application as esterification catalysts for deacidification of crude oil[J];燃料化学学报;2017-09
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2 SUN Wen1,WANG Xiao-li2,ZHAO Zhen-hua1,DING Ke-qiang2, LIU Xian-feng,WU Gong-de2(1 Department of Environment,Hohai University,Nanjing 210024,China; 2 Department of Environment and Technology,Nanjing Institute of Technology,Nanjing 211167,China);Selective Oxidation of Toluene to Benzyl Alcohol Catalyzed by FModified CuNiAl Hydrotalcite Compounds[J];分子催化;2013-01
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