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《Journal of Bijie University》 2008-04
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Synthesis and Crystal Structure of 1,8-Alkylenedipicolininum Dibromide

LV,Jing-Song WU,Ming-Qiang XIAO,Xin TAO,Zhu~* XUE,Sai-Feng ZHU,Qian-Jiang (Chemistry Department of Bijie college,Bijie 551700)(Institute of Applied Chemistry,Guizhou University,Guiyang 550025)  
1,8-alkylenedipicolininum dibromide was synthesized and characterized by ~1H NMR and MS.X-ray single crystal diffraction analysis indicates that the crystal belongs to triclinic system with space group P-l,a=0.97062(3)nm,b=1.04186(4)nm,c=1.32220(4)nm,α=96.028(2)°,β=98.505(2)°,γ= 111.731(2)°,V= 1.20967nm3,Z=2,D_c=1.388 Mg·m~(-3),μ=1.46mm~(-1),F(000)=524.0,The final R= 0.0946,wR=0.3134.
【CateGory Index】: O626.32
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