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《Journal of Baoji University of Arts and Sciences(Natural Science Edition)》 2008-03
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Synthesis of N,N′-bis(x-methoxy salicyl aminal ethylene) oxalamide

ZHANG Mei-li(College of Chemistry and Chemical Engineering,Yan'an University,Yan'an 716000,Shaanxi,China)  
Aim Two new symmetrical oxalamides,Schiff base bridging ligands were designed and synthesized.Methods The final two compounds were synthesized via a series of reaction: diethyl oxalate and ethylenediamine,and then N,N'-bis(2-aminoethyl)-ethylene amide and o-vanillin,vanillin.Results N,N′-bis(3-methoxy salicyl aminal ethylene)oxalamide(H4Lc) and N,N′-bis(4-methoxy salicyl aminal ethylene)oxalamide(H4Ld) were synthesized.Conclusion The composition of compounds H4Lc and H4Ld were identified by elemental analysis,IR spectrum,NMR,UV spectrum and melting point menstruation.
【CateGory Index】: O641.4
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