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《China Surface Engineering》 2007-05
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Investigation on Structure of Microarc Oxidation Ceramic Layer on Titanium Alloy

WANG Qing-liang, XU Ling-li, GE Shi-rong (College of Materials and Engineering, China University of Mining and Technology, Xuzhou 221007, China)  
Microarc oxidation was used to prepare ceramic oxide layer on the surface of Ti6A14V alloy in CaC3H5(OH)2PO4–Ca(CH3COO)2 aqueous solution. The microstructure of the coating was analyzed synthetically. The experimental results showed that a porous ceramic film containing calcium and phosphate on surface of Ti6A14V alloy was acquired. This ceramic film was divided into two films of the inner and outer layers. The thin and compact inner layer contained the equably distributed small holes. The outer layer was thick and porous. The size and depth of these holes increased with an increase of the voltage. Ca and P distibuted unevenly in ceramic film. The content of Ca in inner layer was higher than that in outer layer, but P concentration was almost even in inner and outer layers. And the content of Ca and P was highest in the secondary surface layer. The surface of Ti6A14V alloy after microarc oxidation became rough and a little Ca and P diffused into substrate.
【Fund】: 江苏省自然科学基金(BK2005019);; 中国矿业大学基金项目(2005B032)
【CateGory Index】: TG174.453
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