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《Packaging Engineering》 2008-04
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Synthesis of Quaternary Cationic PVA Membrane Material

GUO Nai-ni1,2,YANG Jian-zhou1(1.Shaanxi University of Science & Technology,Xi'an 710021,China;2.Xianyang Normal University,Xianyang 712000,China)  
Quaternary cationic PVA was synthesized with polyvinyl alcohol(PVA),triethylamine,and epichlorohydrin as raw material by ultrasonic vibration technology.Triethylamine and epichlorohydrin were used to synthesize the intermediate of glycidyl ether of 3 ethyl chloride ammonium(GTA) by water efficient synthesis method.A quaternary cationic PVA polyvinyl alcohol membrane material was prepared by modification of PVA with GTA.The influence of the molar ratio of triethylamine and epichlorohydrin,and the reaction pH on the yield of GTA was studied.The influence of GTA to PVA ratio on the synthesis of quaternary cationic PVA was analyzed.The structure and nitrogen content of the production were analyzed with IR characterization.
【Fund】: 陕西省自然科学基金资助项目(2006B27)
【CateGory Index】: TQ320.721
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