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《Journal of Jiangxi Normal University(Natural Sciences Edition)》 2006-05
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Spectrophotometric Determination of Cationic Surfactants in Water with Coomassie Brilliant Blue G250

QIN Zong-hui~1,TAN Rong~2,FU Wei-quan~3(1.Department of Chemistry and Environmental Sciences,Fuling Normal College,Chongqing 408003,China;2.Fuling Pharmaceutical Factory,Tiji Group,Chongqing 408000,China;3.Chongqing Fuling Fifth Middle School,Chongqing 408000,China)  
HCl-NaOAc buffer medium in pH 3.60,coomassie brilliant blue G250(CBBG) reacts with cationic surfactants(CS) to form an ion-association complex,the colors of solutions change obviously,with the maximum color fading wavelength at 584 nm(CBBG-CTMAB system) and 582 nm(CBBG-CPB system),the fading intensity is also proportional to the concentration of cationic surfactants,a sensitive spectrophotometric method is developed for determination of cationic surfactants.The concentration of CS in the range of 0~1.97×10~(-5) mol/L(CTMAB system) and 0~2.31×10~(-5) mol/L(CPB system) obeys Beer' law at the maximum color fading wavelength,the apparent molar absorptivity is 1.64×10~4 L/(mol·cm)(CTMAB system) and 1.31×10~4 L/(mol·cm)(CPB system),the detection limit is 8.03×10~(-7) mol/L(CTMAB system) and 1.02×10~(-6) mol/L(CPB system).The method has high sensitivity and fairly good selectivity.The method is applied to the determination of CS in water samples,with satisfactory results.
【Fund】: 重庆市第二批中青年骨干教师资助计划项目〔渝教人(2005)2号〕
【CateGory Index】: X832
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