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《China Surfactant Detergent & Cosmetics》 2003-03
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Application of the gemini quaternaries containing ester-bond surfactants in the determination trace aluminium

SUN Hong1,ZHANG Ze2,JIA Li-hua1(1.Chemical and Chemistry Engineering College of Qiqihar University, Qiqihar161006, China;2Qiqihar Environmental Monitorin Station, Qiqihar161005, China)  
The impact of gemini ester-bond containing quaternary ammonium surfactants(EDC) on the complex system of aluminium-chrome-azurol S(CAS)was studied by UV-VIS spectrophotometry. In a acetate buffer solution(pH 68),with the presence of methyl orange?o-phenanthroline and ascorbic acid,aluminium can react with CAS and form a blue-violet complex whose maximum absorption was 646 nm and whose molar absorptivity was 103×105 L·mol-1·cm-1.The influnence of cetyltrimethyl ammonium bromide (CTMAB)on aluminium-chrome-azurol S was determined.The linearity range of Al3+ is 02 mg/L~10 mg/L.The recovery is 95 %.The relative standard deviation is 38 %.The method can be used to determine trace aluminium in water.
【Fund】: 黑龙江省普通高等学校骨干教师创新能力资助计划(2003)
【CateGory Index】: O657.3
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