Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《China Surfactant Detergent & Cosmetics》 2005-01
Add to Favorite Get Latest Update

Preparation of complex catalyst SO~(2-)_4/ZrO_2-TiO_2 and its application in reaction for synthesis of alkyl polyglucoside

YU Bing-chuan,WU Hong-te,ZHU Zhong-jun(College of Chemistry and Environmental Engineering,Yangtze University,Jingzhou434025,China)  
A complex catalyst system,SO~(2-)_4/ ZrO_2-TiO_2 was prepared and used in the reaction for the synthesis of alkyl polyglucoside(APG).The optimal conditions for the catalyst preparation are,calcination temperature,500 ℃~550 ℃,concentration of H_2SO_4 in the impregnating solution,(0.5 mol/L)~0.55 mol/L and EDTA dosage,5 %(w/%)of the catalyst.Conditions for the APG synthesis are,mass ratio of the catalyst against glucose added,0.015∶1~0.020∶1,reaction time,3.5 h,yield(w/% of APG against glucose),150 %.The product has a pale yellow color,D.P,1.46,cmc,0.006 5 %,with good foaming power,foam stability achieves 82.2 %(1 h).The catalyst can be reused for 5 times.
【Fund】: 长江大学科研基金资助项目(HNZDi200307)
【CateGory Index】: TQ423.2
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【References】
Chinese Journal Full-text Database 10 Hits
1 WU Hongte*,YU Bingchuan,GE Shengxiang(College of Chemistry and Environmental Engineering,Yangtze University,Jingzhou 434023,Hubei,China);Synthesis of glycerol triacetate over composite solid super acid catalyst SO_4~(2-)/ZrO_2-TiO_2[J];Industrial Catalysis;2007-08
2 WU Hong-te,YU Bing-chuan,GE Sheng-xiang(College of Chemistry and Environmental Engineering,Yangtze University, Jingzhou 434023,China);The Synthesis of Di-2-ethylhexyl Maleate Catalyzed by Complex Solid Superacid SO_4~(2-)/ZrO_2-TiO_2[J];Chemistry & Bioengineering;2007-05
3 WU Hong-te,YU Bing-chuan,GE Sheng-xiang(College of Chemistry and Environmental Engineering,Yangtze University,Jingzhou 434023,China);Synthesis of Di-2-ethylhexyl Adipate Catalyzed by Complex Solid Super Acid SO_4~(2-)/ZrO_2-TiO_2[J];Chemistry & Bioengineering;2007-09
4 YU Bing-chuan,WU Hong-te(College of Chemistry and Environmental Engineering,Yangtze University,Jingzhou 434025,China);Synthesis of Tributyl Citrate Catalyzed by Compound Solid Superacid SO_4~(2-)/ZrO_2-TiO_2[J];Chemistry & Bioengineering;2010-11
5 WU Hongte,YU Bingchuan,GE Shengxiang (School of Chemistry and Environmental Engineering,Yangtze University,Jingzhou 434023,Hubei,China);Complex solid super acid SO_4~(2-)/ZrO_2-TiO_2 used in synthesis of glycerol triacetate[J];Chemical Industry and Engineering Progress;2007-07
6 YANG Chun-hua LIU Li-ping Jilin Vocational College of Industry and Technology, Chemical Engineering Dept, Jilin 132013 China Jilin GuangDa Electric Power Equipment Company Jilin Ltd, Jilin 132013 China;Development and Applications of SO_4~(2-)/MxOySolid Superadd Catalyst[J];Technique & Education;2005-02
7 HOU Qi-jun (State Key Laboratory of Fine Chemicals, Dalian University of Technology, Dalian 116012, China);Greening of Surfactant Industry[J];Fine and Specialty Chemicals;2008-19
8 WU Hong-te,YU Bing-chuan,GE Sheng-xiang (College of Chemistry and Environmental Engineering,Yangtze University,Jingzhou 434023,Hubei,China);Synthetic Method of Methyl 1-Naphthylacetate on Complex Solid Super Acid Catalyst SO_4~(2-)/ZrO_2-TiO_2[J];Agrochemicals;2007-06
9 DAI Yu-gong,LU Yan(School of Chemical and Environmental Enginering,Shanghai Institute of Technology,Shanghai 200235,China);Study on the Synthesis of Dodecyl Glucoside Catalyzed by SO_4~(2-)/ZrO_2-La_2O_3[J];Journal of Shanghai Institute of Technology(Natural Science);2011-03
10 Yu Bing-chuan Wu Hong-te (College of Chemistry and Environmental Engineering, Yangtze University, Jingzhou, 434025);Synthesis of Di(2-ethyl hexyl) Phthalate Catalyzed by Compound Solid Superacid SO_4~(2-)/ZrO_2-TiO_2[J];Plastics Additives;2010-05
【Citations】
Chinese Journal Full-text Database 9 Hits
1 Yu Tao JING Guo lin (Department of petrochemical engineering,Daqing petroleum institute Anda 151400,China);Preparation of the Surfactant Alkyl Polyglucoside from Starch[J];CHINA SURFACTANT DETERGENT & COSMETICS;2000-02
2 FAN Li Juan LIN Qiang (Institute of Chemical Engineering,Beijing United University,Beijing 100023,China);The New King of Catalysts for the Synthesis of Alkyl-Polyglycoside[J];China Surfactant Detergent & Cosmetics;2001-05
3 LIU Xiao jun, Yu Guang suo, WANG Yi fei,YU Zun hong (Institute of Clean Coal Technology, East China University of Science & Technology, Shanghai 200237, China);Advances in SO_4~(2-) /M_xO_y inorganic solid superacids[J];Gongye Cuihua (Industrial Catalysis);2001-06
4 WANG Zhiliang,CHEN Xuemei;Technical progress on the synthesis of alkyl polyglycoside[J];JOURNAL OF CHEMICAL INDUSTRY & ENGINEERING;2000-03
5 OUYANG Xin ping,QIU Xue qing,LAN Ren hua,YANG Zhuo ru,CHEN Huan qin (Research Institue of Chemical Engineering,South China University of Technology,Guangzhou 510641,China);Study of Infrared Spectrograms of Dodecyl Polyglycosides[J];Fine Chemicals;2001-03
6 Fang Zhijie, Mao Wenyong, Liao Fengmei, Jiang Aiqin, Sun Dongping and Lu Lude (Chemical Engineering School, Nanjing University of Science & Technology, 210094);THE PREPARATION OF SOLID ACID TiO_2/SO_4~(2-) AND TiO_2-ZrO_2/SO_4~(2-) AND ITS APPLICATION IN SYNTHESIS OF ALKYLPOLYGLYCOSIDE[J];SPECIALITY PETROCHEMICALS;2000-02
7 LUO Fang,?XIN Xiao yan (College of Chemical and Light Industrial Engineering,Yunnan Industry University,Kunming 650051, China);SYNTHESIS OF ALKYL-POLYGLYCOSIDE CATALYZED BY SOLID ACID[J];CHEMISTRY AND INDUSTRY OF FOREST PRODUCTS;2000-01
8 JiangAiqin FangZhijie SunDongping ZhaoChengfang YeZhiwen (School of Chemical Engineering,NUST,Nanjing 210094);Synthesis of Alkylpolyglucoside by Using Solid Acid as Catalyst[J];JOURNAL OF NANJING UNIVERSITY OF SCIENCE AND TECHNOLOGY;2000-04
9 GU Xu-peng, CHEN Tong-yun (Department of Chemical Engineering, Anhui Polytechnic University, Maansan 243002, China);A Study of the Improvement in the Method for Synthesizing Alkye Polyglucosides and Its Application[J];Journal of Applied Sciences;2001-04
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 YUAN Hao1,YANG Xue-jie2,ZHANG Ping1,Zhao Wei-jun1(1.College of Chemical Engineering,Guizhou University,Guiyang 550003,China; 2.Guizhou Light Industry Technical College,Guiyang 550003,China);Synthesis of Starch-based Glycol Polyglucoside[J];Anhui Chemical Industry;2007-01
2 ZHANG Liping(Department of Chemical Engineering, Daqing Vocational College, Daqing 163254,China);Synthesis of Alkyl Polyglycoside and the Development of Its Application[J];Journal of Daqing College;2004-04
3 YANG Ke-er,QIU Hong-hua,TONG Shan-ling,YAN YanDepartment of Chemistry,Shantou University,Shantou,515063,Chin;New Preparation Method and Catalytic Activity of Solid Superacid SO_4~(2-)/TiO_2 in Esterification to Form Dibutyl Phthalate[J];Journal of Molecular Catalysis;2005-05
4 Gao Nan,Zhang Chunhua,Zhang Zongjian(Central Research Institute of China Chemical Science and Technology,Beijing 100083,China);The application of green surfactants in pesticide formulation[J];Engineering Sciences;2009-04
5 Liu Qunying,Zhou Wenfu(Departmenent of Chemical and Bio-Engineering,SanMing College,FuJian 365004,China);On the Synthesis of Alkyl Polyglucoside by One-Stepwith Charcoal Sulfoacid Catalyst[J];Guangdong Chemical Industry;2010-02
6 LU Xing-lian,WANG Qing-ning,KANG Wen-shu(College of Petrochemical Technology,Lanzhou Univ.of Tech.,Lanzhou 730050,China);Study of synthesis processing of alkyl polyglycosides from oleaster sugar[J];;2005-06
7 YU Shaoming,HAO Wenzheng,WANG Hualin,LU Yaling,ZHAI Linfeng,SHI Tiejun (School of Chemical Engineering , Hefei University of Technology, Hefei 230009, China);PREPARATION AND CATALYTIC PERFORMANCE OF MIXED Zr/Al PILLARED CLAY SOLID SUPERACID[J];Journal of the Chinese Ceramic Society;2007-10
8 LIU Xiao jun, Yu Guang suo, WANG Yi fei,YU Zun hong (Institute of Clean Coal Technology, East China University of Science & Technology, Shanghai 200237, China);Advances in SO_4~(2-) /M_xO_y inorganic solid superacids[J];Gongye Cuihua (Industrial Catalysis);2001-06
9 LI Qiu-rong,ZHAO Qian(School of Environmental and Chemical Engineering,Yanshan University,Qinhuangdao 066004,Hubei,China);Synthesis of n-butyl acetate catalyzed by solid S_2O_8~(2-)/TiO_2 superacid[J];Industrial Catalysis;2006-07
10 WU Hongte*,YU Bingchuan,GE Shengxiang(College of Chemistry and Environmental Engineering,Yangtze University,Jingzhou 434023,Hubei,China);Synthesis of glycerol triacetate over composite solid super acid catalyst SO_4~(2-)/ZrO_2-TiO_2[J];Industrial Catalysis;2007-08
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 Chen Yonghong(Dept. Of chemistry, Huai Nan Normal Institute);Advance on Catalysts of Esterify Reactions[J];JOURNAL OF ANHUI AGROTECHNICAL;1998-01
2 Sun Wenxian,Yang Haizhen,Wang Shaoping(School of Environmental Science and Engineering,Tongji University,Shanghai 200092,China);A Review of Degradation of Phthalate Esters[J];Environmental Science and Management;2008-03
3 LI Juan~1 YAN Shi-cheng~2 LI Jian-wei~1 CHEN Biao-hua~1 DENG Wei~1(1.State Key Laboratory of Chemical Resource Engineering,Beijing University of Chemical Technology,Beijing 100029,China;2.Jilin Vocational College of Industry and Technology,Jilin 132000,China);Dodecylbenzene synthesis by the alkylation of benzene with 1-dodecene over mesoporous zeolites[J];Journal of Beijing University of Chemical Technology(Natural Science Edition);2006-06
4 LI Yu,HUANG Guo-chao(Guangdong Industry Technical College,Guangzhou 510300,China);Microwave Assisted Synthesis and Application of Cinnamic Esters on Packaging Materials[J];Packaging Engineering;2007-02
5 Yu Tao JING Guo lin (Department of petrochemical engineering,Daqing petroleum institute Anda 151400,China);Preparation of the Surfactant Alkyl Polyglucoside from Starch[J];CHINA SURFACTANT DETERGENT & COSMETICS;2000-02
6 LIAN Wei LAN Ren hua OUYANG Xin ping CHEN Huan qin (Research Institute of Chemical Engineering, South China University of Technology,Guangzhou 510641,China);The Colour of Alkyl Polyglycosides and Decolored[J];China Surfactant Detergent & Cosmetics;2001-03
7 FAN Li Juan LIN Qiang (Institute of Chemical Engineering,Beijing United University,Beijing 100023,China);The New King of Catalysts for the Synthesis of Alkyl-Polyglycoside[J];China Surfactant Detergent & Cosmetics;2001-05
8 XI Li-min~(1,2),REN Qi-long~2(1.Taizhou Technical College,Departement of Biological and Chemical Engineering,Taizhou 318000,China;2.Zhejiang University,National Laboratory of Secondary Resources Chemical Engineering,Hangzhou 310027,China);Preparation of fatty acid methyl ester catalyzed by solid acid from by-products of plam oil[J];China Surfactant Detergent & Cosmetics;2006-06
9 LI Gong 1,2, KAN Qiubin 1, TONG Huijuan 2, WU Tonghao 1*, XU Ning 1, WU Peng 1, WANG Dongyang 1 (1 College of Chemistry, Jilin University, Changchun 130023, Jilin, China; 2 Department of Chemical Engineering,Jiangsu Polytechnic University, Changzhou 213016, Jiangsu, China);Catalytic Performance of Nanometer MCM-49 Zeolite for Alkylation Reaction of Benzene with 1-Dodecene[J];Chinese Journal of Catalysis;2004-10
10 YU Hui,ZHU Yinhua,LIU Chang,YANG Zhuhong,LU XiaohuaFENG Xin State Key Laboratory of Materials-Oriented Chemical Engineering,Nanjing University of Technology,Nanjing 210009,Jiangsu,China;Preparation of Novel Mesoporous SO_4~(2-)/TiO_2 Solid Acid Catalyst and Its Catalytic Activity for Esterification[J];Chinese Journal of Catalysis;2009-03
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 CHEN Shi-jie(Changzhou LGJ Vocational Technology College,Changzhou 213004,China);Alkyl Polyglycoside——A New Type Green Surfactant[J];Anhui Chemical Industry;2010-02
2 ZENG Lei~*, ZHOU Congwen, WANG Delian, PENG Lan (Hunan Environment & Biological Polytechnic College, Hengyang 421005, Hunan, China);Transesterification of rape oil and glycol catalyzed by clay-supported TiO_2-SO_4~(2-)[J];Industrial Catalysis;2010-03
3 ;Research Progress on the Synthesis of Glyceryl Ester Compounds[J];Popular Science & Technology;2012-11
4 YU Bing-chuan,WU Hong-te(College of Chemistry and Environmental Engineering,Yangtze University,Jingzhou 434025,China);Synthesis of Tributyl Citrate Catalyzed by Compound Solid Superacid SO_4~(2-)/ZrO_2-TiO_2[J];Chemistry & Bioengineering;2010-11
5 LI Zhaohui,HOU Shu'en,ZHAO Xinying,HUANG Yujuan,WANG Fengxiang (School of Material Science & Chemical Engineering,China University of Geosciences,Wuhan 430074,Hubei,China);Synthesis of comb-like polycarboxylate based superplasticizer catalyzed by solid superacid SO_4~(2-)/Zr~(4+)[J];Chemical Industry and Engineering Progress;2010-03
6 LIANG Zi-jia,WEI Lin-yan,YUE-Yi,ZHANG-Yang,ZHANG Shou-cai,LI Chuan-bi (Institute of Chemical ,Jilin Normal University,Siping 136000 ,China);Preparation of Biodiesel with Solid acid Catalyst (SO_4)~(2-)/ ZrO_2-SnO_2[J];Hebei Chemical Engineering and Industry;2009-01
7 Tian Mengchao, Feng Xilan, Feng Yichang (1.Zhongyuan University of Technology, Zhengzhou 450007,China; 2.Henan Institute of Science and Technology,Xinxiang 453003,China);Catalytic Synthesis of DIOA by Solid Super Acid Ni~(2+)-SO_4~(2-)/ZrO_2-Al_2O_3[J];Journal of Henan Institute of Science and Technology;2009-04
8 WANG Qing-ning,SONG Ying,ZHANG Fei-long,ZHUO Xian-zhen,ZHAO Qiu-ping (School of Petrochemical Engineering,Lanzhou University of Technology,Lanzhou 730050,China);Synthesis and properties of polyglycosides from sweet potato starch[J];Science & Technology in Chemical Industry;2010-02
9 XIE Cong-xia1, YU Shi-tao2 , LIU Shi-wei 2,3, LIU Fu-sheng2, LI Hong-juan2, LI Lu2(1. College of Chemistry and Molecular Engineering,Qingdao University of Science and Technology, Qingdao 266042, China;2. College of Chemical Engineering,Qingdao University of Science and Technology, Qingdao 266042,China; 3. Institute of Chemical Industry of Forest Products,CAF;Key and Open Lab. on Forest Chemical Engineering,SFA, Nanjing 210042, China);Research Situation on Deep Processing of the By-product Glycerin from Biodisesl Production[J];Biomass Chemical Engineering;2008-04
10 WU Liang-biao,LENG Bao-ling (Department of Petrochemical,Lanzhou College of Petrochemical Technology,Gansu Lanzhou 730060,China);Catalytic Synthesis of Glyceryl Triacetate With H_2SO_4-K_2Cr_2O_7 Modified Activated Carbon[J];Liaoning Chemical Industry;2011-06
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 Luo Xiquan;Performances of A New Generation Surfactants──Alkyl Polyglucosides and Its Application in Household Chemical Industry[J];SURFACTANT INDUSTRY;1998-01
2 ;Analysis of Alkyl Glycosidesby GC[J];China Surfactant Detergent & Cosmetics;1991-06
3 $ Gao Genzhi (Chemistry Department, Qufu Normal University, Qufu 273165) Yu Shitao, Yang Jinzong (Department of Fine Chemicals, Dalian University of Technology, Dalian 116012);PREPARATION OF SO 2- 4/TiO 2 Al 2O 3 SnO 2 AND ITS CATALYTIC PROPERTIES FOR THE SYNTHESIS OF DIOCTYL ADIPATE[J];CHINESE JOURNAL OF CATAL YSIS;1996-01
4 Zeng Jianqing, Zhong Bing, Luo Qingyun, Wang Qin, Xiang Hongwei (Institnte of Cool Chemistry, Chinese Academy of Sciences, Taiyuan 030001);Preparation of SO_4~(2-)/ZrO_2 Superacid Catalyst by Crystalline Superfine ZrO_2[J];Journal of Molecular Catalysis;1993-06
5 LIAO Shijun YANG Zhaoxi ZHANG Xiaoling LIU Ying(Department of Applied Chemistry, South China University of Technology Guangzhou 510641)WANG Lefu HUANG Zhongtao(Department of Chemical Engineering, South China University of Technology Guan;Preparation of Catalyst SO_4~(2-)/ZrO_2SiO_2 and Its Catalysis for Esterification of Acetic Acid with Butanol[J];JOURNAL OF MOLECULAR CATALYSIS (CHINA);1998-01
6 Hu Fei Wen Qibiao (Light Chemical Ind. Inst.,Science and Technology University of Southern China Guangzhou 510641);Development of Surfactant Derived from Starches[J];GUANGXI CHEMICAL INDUSTRY;1997-01
7 Lu Weijing (Dept. of Chemical Engineering, Guangxi University Nanning 530004);Preparation, Property and Application of Alkyl Polyglycoside[J];GUANGXI CHEMICAL INDUSTRY;1997-01
8 MIAO Chang-xi(Shanghai Research institute of Petrochmical Technology, Shanghai 201208, China)GAO Zi(Department of Chemistry, Fudan University, Shanghai 200433, China);Influence of addition of Al_2O_3 on property of SO_4~(2-)/ZrO_2 solid superacid[J];GONGYE CUIHUA (INDUSTRIAL CATALYSIS);1999-05
9 HUANG Bi chun (Dept Chem Eng,South China Univ Technol,Guangzhou 510641,China);The acidity and catalytic properties of solid superacid SO_4~(2-)-MoO_3-ZrO_2 for esterification[J];GONGYE CUIHUA (INDUSTRIAL CATALYSIS);2000-02
10 Yang Zhenbao, Yang Jinzong(Department of Fine Chemicals, Dalian University of Technology, Dalian, 116012);Alkyl Glycoside——Novel World-Class Surfactant[J];Chemical Industry and Engineering Progress;1993-01
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved