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《China Surfactant Detergent & Cosmetics》 2006-06
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Preparation of fatty acid methyl ester catalyzed by solid acid from by-products of plam oil

XI Li-min~(1,2),REN Qi-long~2(1.Taizhou Technical College,Departement of Biological and Chemical Engineering,Taizhou 318000,China;2.Zhejiang University,National Laboratory of Secondary Resources Chemical Engineering,Hangzhou 310027,China)  
Fatty acid methyl esters were prepared by esterification in a fixed bed reactor from methanol and fatty acids in palm oil deodorizer distillate(PODD) using a cation exchange resin as catalyst.Experimental results showed that the optimum mass ratio for the esterification was n(methyl alcohol)/n(PODD)=17.3.The conversion of fatty acids increases with the temperature when the temperature was below the boiling point of methanol.The conversion increases with time as well,but the increasing rate declines with time.The conversion achieves 87% at 64 ℃,56 min.
【Fund】: 浙江省科技计划重点资助项目(001103231)
【CateGory Index】: TQ645.1
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