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《Chinese Journal of Catalysis》 2004-09
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Preparation of NiW/Al_2O_3 Hydrodesulfurization Catalyst by Ultrasound-Microwave Treatment

LIU Xuefen *, ZHANG Le, SHI Yahua, NIE Hong, LONG Xiangyun(Research Institute of Petroleum Processing, SINOPEC, Beijing 100083, China)  
Hydrotreating is one of the important means for the production of clean fuels and its efficiency largely depends on the hydrotreating catalysts. The preparation methods greatly influence the nature of the catalysts and result in different activity, selectivity and stability. In the present study, the NiW/Al 2O 3 catalyst was prepared by impregnation combined with ultrasound treatment and microwave drying. The catalytic properties, surface state and morphology of the catalyst were examined by using thiophene hydrodesulfurization, XPS and TEM techniques, respectively. The as-prepared catalyst exhibited higher hydrodesulfurization activity than that obtained by the conventional method. The XPS and TEM analysis revealed that combination of the ultrasound treatment and microwave drying could promote the sulfuration and surface dispersion of the active metals and produce more unsaturated "rim" and "edge" sites in the WS 2 slabs. As a result, the hydrodesulfurization activity of the as-prepared catalyst was remarkably enhanced.
【CateGory Index】: TE624.9
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