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《Chinese Journal of Catalysis》 2004-11
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Synthesis of Ti-Containing MCM-41 Mesoporous Molecular Sieve in the Presence of Ammonia

ZHAO Wenjuan, HE Bin, ZHANG Jinlong *(Institute of Fine Chemicals, East China University of Science and Technology, Shanghai 200237, China)  
Ti-doped MCM-41 mesoporous molecular sieve was synthesized in the presence of ammonia using TiCl 3 as titanium source and TEOS as silica source. The synthesis method was simple, and it needed neither auxiliary templates nor alcohols. The molecular sieve was characterized by XRD and N 2 adsorption/desorption isotherms techniques. The results showed that the synthesized MCM-41 had hexagonal mesostructure with long-range order and good crystallinity. UV-Vis spectra indicated that four clear absorption peaks appeared in the range of 200~300 nm, which gave the facts that there existed different forms of Ti atoms doped in the framework of Ti-MCM-41.
【Fund】: 国家自然科学基金 ( 2 0 0 73 0 2 6);; 上海市教育发展基金会资助项目
【CateGory Index】: O643
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