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《Chinese Journal of Catalysis》 2005-04
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Catalytic Feature of Ni/MgO Catalyst for CO_2 Reforming of Methane under Pressurized Condition

WANG Yuhe 1,2, XU Boqing 1*(1 Innovative Catalysis Program, Key Laboratory of Organic Optoelectronics and Molecular Engineering,Department of Chemistry, Tsinghua University, Beijing 100084, China; 2 Department of Chemistry,Heilongjiang,Harbin Normal University, Harbin 150080, Heilongjiang, China)  
The Ni/MgO-AN catalyst, prepared by loading of Ni onto nano-magnesia (MgO-AN) obtained from thermal processing of a Mg(OH)_2 alcogel, was used for CO_2 reforming of methane under different pressures (0.1~2.0 MPa). The catalyst exhibited high and stable activity under atmospheric pressure. However, the catalyst activity declined with increasing reaction pressure. Thermogravimetry, X-ray diffraction and temperature-programmed hydrogenation (TPH) characterization results showed that carbon deposition was very little on the catalyst reacted under atmospheric pressure. In contrast, serious carbon deposition was found on the catalyst reacted under 1.0~2.0 MPa. The amount of carbon deposits increased with the reaction time up to 12 h when it became stabilized, indicating a self-stabilization feature of the working catalyst at the high pressures. No significant sintering of metallic nickel was detected on the used catalyst in the reaction under atmospheric pressure whereas marked sintering happened in the high-pressure reaction. The carbon deposits on the catalyst used in the atmospheric pressure reaction appeared as a single peak on the TPH profile, but two peaks were observed for the samples used in the high-pressure reaction. These results demonstrate that the catalytic performance of Ni/MgO-AN was different under atmospheric and high pressures.
【Fund】: 国家自然科学基金(20073023);; 国家杰出青年基金(20125035)资助项目.
【CateGory Index】: O643
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