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《Chinese Journal of Catalysis》 2005-04
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Characterization and Catalytic Performance of Co/HMS and Co/SiO_2 Catalysts for Fischer-Tropsch Synthesis

YANG Wenshu 1,2*, FANG Dingye 1, XIANG Hongwei 2, LI Yongwang 2, LIU Jisen 1(1 College of Chemical Engineering, East China University of Science and Technology, Shanghai 200237, China;2 State Key Laboratory of Coal Conversion, Institute of Coal Chemistry, The ChineseAcademy of Sciences, Taiyuan 030001, Shanxi, China)  
The 15%Co/HMS and 15%Co/SiO_2 catalysts were prepared by incipient wet impregnation and characterized by N_2 adsorption-desorption, XRD, XPS, TPR and TG. The amorphous SiO_2 used was derived from HMS in boiling water for 12 h. The strong metal-support interaction for the Co/HMS catalyst was affirmed by TPR and XPS. The Co_3O_4 crystallite size of the oxidized Co/HMS catalyst was smaller than that of the oxidized Co/SiO_2 catalyst. XRD results indicated the location of partial cobalt oxide crystallites on the external surface of the oxidized Co/HMS and Co/SiO_2 catalysts. Mesoporous pores were blocked by cobalt oxide for the oxidized Co/HMS according to the N_2 adsorption-desorption. The Co/HMS catalyst presented higher F-T activity owing to the better cobalt dispersion and appropriate cobalt reduction. Under the conditions of V(H_2)/ V(CO)=2.0, GHSV=500 h -1 and p=2.0 Pa, the CO conversion over Co/HMS was kept about 85%, and the methane selectivity of about 8.0% and C_ 5~C_ 18 hydrocarbon selectivity of 70% were obtained as the reaction temperature increased from 473 to 493 K. Reduction for a long time (16 h) before reaction led to the sintering and agglomeration of cobalt crystallites in Co/SiO_2, so that the F-T activity became lower. The CO conversion over Co/SiO_2 gradually increased from 66% to 98% when the reaction temperature increased from 503 to 523 K, but the hydrocarbon distribution was not so good as that over Co/HMS.
【Fund】: 国家重点基础研究发展规划(G1999022402);; 山西省自然科学基金(20021024)资助项目.
【CateGory Index】: O643
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