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《Chinese Journal of Catalysis》 2005-09
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Low-Temperature Hydrothermal Synthesis of TiO_2 Photocatalyst with High Activity

YU Jiaguo*, XIONG Jianfeng, CHENG Bei ( State Key Laboratory of Advanced Technology for Material Synthesis and Process ing,Wuhan University of Technology, Wuhan 430070, Hubei , China)  
Anatase TiO2 nanocrystal photocatalyst with high activity was prepared using T i(SO4)2 and CON2H4 as raw materials by a simple hydrothermal method at l ow temperature. The as-prepared samples were characterized by X-ray diffract ion (XRD), scanning electron microscope (SEM) and N2 adsorption-desorption. T he photocatalytic activity of the samples was evaluated using the photocatalytic oxidation of acetone in air at room temperature. It was found that hydrothermal treatment could obviously promote the crystallization of TiO2 at low temperat ure without heat-treatment. TiO2 powders prepared by this method at 160 ℃ fo r 3 h or 180 ℃ for 2 h showed good activity for the photocatalytic oxidation of acetone and the photocatalytic activity of as-prepared TiO2 powders exceede d that of Degussa P25 by a factor of more than 3 times. This might be attributab le to the fact that the as-prepared TiO2 powders had large specific surface a rea and small crystallite size.
【Fund】： 国家自然科学基金(50272049 20473059);; 教育部优秀青年教师资助计划;; 教育部留学回国人员科研启动基金;; 材料复合新技术国家重点实验室重点基金(WUT2004Z03)资助项目.
【CateGory Index】： O643.36
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