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《Chinese Journal of Catalysis》 2006-10
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Preparation,Characterization,and Photocatalytic Activity of Visible Light Driven Chlorine-Doped TiO_2

CHEN Heng,LONG Mingce,XU Jun,CAI Weimin~*(School of Environmental Science and Engineering,Shanghai Jiao Tong University, Shanghai 200240,China)  
A novel chlorine-doped titanium dioxide catalyst with visible light response was prepared by hydrolysis of tetrabutyl titanate in hydrochloric acid.The catalyst samples were characterized by(X-ray) diffraction,transmission electron microscopy,(X-ray) photoelectron spectroscopy(XPS),and ultraviolet-visible diffuse reflectance spectroscopy.The results showed that the doped element of Cl lowered the temperature of phase transformation of TiO_2 from amorphous to anatase and from anatase to rutile.The absorption edge of chlorine-doped TiO_2 calcined at 300 ℃ shifted to the visible light region.XPS results proved that chlorine existed in the TiO_2 crystal lattice as an anion.The photocatalytic degradation of phenol showed that under visible light(λ400 nm) irradiation,the chlorine-doped TiO_2 photocatalyst calcined at 300 ℃ displayed the best performance,and the degradation ratio of phenol was 42.5% after 120 min.
【Key Words】: titanium dioxide chlorine doped visible light photocatalysis phenol
【Fund】: 高等学校博士学科点专项科研基金(20050248015)资助
【CateGory Index】: O643.36;O614.411
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