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《Chinese Journal of Catalysis》 2008-06
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Catalytic Activity of Nano-V_2O_5/ZnO Photocatalyst for Degradation of Nonylphenyl Poly(oxyethylene)ether

HU Lili,DU Zhiping,TAI Xiumei,LI Qiuxiao,ZHAO Yonghong(China Research Institute of Daily Chemical Industry,Taiyuan 030001,Shanxi,China)  
The nano-V2O5/ZnO photocatalyst samples with different V2O5 contents were prepared by the ammonia immersion method.The crystal structure,specific surface area,particle morphology,surface composition,and spectral characteristics were analyzed by X-ray diffraction,N2 adsorption,transmission electron microscopy,X-ray photoelectron spectroscopy,and diffuse reflectance ultraviolet-visible spectroscopy,respectively.The catalytic activity of the V2O5/ZnO photocatalyst samples for degradation of nonylphenyl poly(oxyethylene)ether(NPE-10) was measured under the irradiation with ultraviolet light and visible light.The crystal size of V2O5/ZnO decreased but its specific surface area increased slightly with the increase of V2O5 content.Compared with the nano-ZnO,the binding energy of V 2p in V2O5/ZnO decreased,but the binding energy of Zn 2p and O 1s increased.The amounts of hydroxyl oxygen and adsorbed oxygen on the V2O5/ZnO surface increased remarkably in contrast to those of the ZnO sample.The catalytic activity of the 2.5% V2O5/ZnO photocatalyst(where 2.5% means n(V)/n(Zn) value) was the highest,and the degradation rate of NPE-10 was about 79% and 61% under the irradiation of ultraviolet light and visible light for 3 h,respectively.
【Fund】: 山西省科技攻关项目(2006031043);; 山西省青年基金项目(2006021012);; 山西省国际合作项目(051012)
【CateGory Index】: O643.32
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