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《Chinese Journal of Catalysis》 2009-02
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Photocatalytic Activity of K_2La_2Ti_3O_(10) Doped with Boron for Hydrogen Production from Water Splitting

YANG Yahui1,2, CHEN Qiyuan1, LI Jie1(1 College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, Hunan, China; 2 College of Minerals Processing and Bioengineering, Central South University, Changsha 410083, Hunan, China)  
The layered perovskite type oxides, K2La2Ti3O10 and K2La2Ti3O10 doped with B, were prepared by the sol-gel method and characterized by power X-ray diffraction and UV-vis diffuse reflectance spectroscopy. The photocatalytic activity of K2La2Ti3O10 and K2La2Ti3O10 doped with B for water splitting was investigated with I- as the electron donor under ultraviolet and visible light irradiation. The electronic structure of K2La2Ti3O10 doped with B was analyzed by the first principle calculations, which reveals the photo responses in the visible region and the improvement of the photocatalytic activity of K2La2Ti3O10. Conclusions were made that K2La2Ti3O10 doped with B exhibited higher photocatalytic activity for hydrogen production. The optimum doping concentration of B was 0.01∶1 (B∶Ti), and the ultraviolet hydrogen production rate was 157.1 μmol/(L·h), which was raised by 166% compared with undoped K2La2Ti3O10. The optimum doping concentration of B was 0.02∶1 (B∶Ti), and the visible hydrogen production rate was 85.2 μmol/(L·h), being 5.2 times that undoped K2La2Ti3O10.
【Fund】: 国家高技术研究发展计划(863计划 2002AA327140);; 湖南省自然科学基金(08JJ3022);; 湖南省科技计划(08FJ4105)
【CateGory Index】: TQ116.2
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