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《Materials Review》 2005-09
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Study on Conditions of Synthesizing NiMgAl Hydrotalcite-like Compounds

SHEN Yanming WU Jing School of Chemical Engineering,Dalian University of Technology,Dalian 116012; Department of Chemical Engineering,Shenyang Institute of Chemical Teachnology,Shenyang 110142 ZHANG Hui ZHANG Zhenxiang Department of Chemical Engineering,Shenyang Institute of Chemical Teachnology,Shenyang 110142 LIU Changhou School of Chemical Engineering,Dalian University of Technology,Dalian 116012;  
NiMgAl hydrotalcite-like compounds with different Ni/Mg/Al molar ratios were synthesized by co- precipitation.The titration curve of simplex and the mixed solutions with different Ni/Mg/Al molar ratios were deter- mined.The effects of precipitation method,crystallized temperature,crystallized time and Ni/Mg/Al molar ratio on the structure of NiMgAl-HTLcs were investigated.Then the synthesized compounds were characterized by XRD,IR.The results showed that the pure NiMgAl-HTLcs phase can be obtained by constant pH method at the pH value ranging from 8 to 9,(Mg+Ni)/Al molar ratio is 1 to 3,Mg/Ni molar ratio is 8 to 16 and crystallized temperature,and crystal- lized time is 65℃ and 6h respectively.It is also founded that the synthesized hydrotalcite-like compounds are more inte- grated with the increasing of(Mg+Ni)/Al molar ratio and the interlayer-spacing decreased with the increasing of Mg/ Ni molar ratio.
【Fund】: 沈阳化工学院中青年科研启动基金项目(3200602270)
【CateGory Index】: TB321
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