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《Journal of Materials Science and Engineering》 2007-01
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Preparation of Ultrafine Plate-like WO_3 via W/O Microemulsions Method

SONG Tao,QIU Tai,SHEN Chun-ying,LI Zhi-shun,CHEN Xiao-jie(College of Materials Science and Engineering,Nanjing University of Technology, Nanjing 210009,China)  
Ultrafine plate-like WO_3 was synthesized in quaternary W/O microemulsion solution containing TritonX-100,cylcohexane,hexanol and water.XRD patterns show that the ultrafine sheets are the mixture of monoclinic and triclinic WO_3 crystals.SEM images show that the as-synthesized samples are homogeneous grain-size ultrafine sheets.BET analysis show that the ultrafine plate-like WO_3 has large specific area.Two key variables-ω_0(molar ratio of water to surfactant)and reactant concentration in water were investigated to reveal the size and shape changing of ultrafine plate-like WO_3.The mechanics of ultrafine plate-like WO_3 prepared in TritonX-100/cylcohexane/exanol /water solution was discussed tentatively.
【Fund】: 国防新材料重点资助项目(MKPT-05-211)
【CateGory Index】: TB383.1
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