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《Journal of Materials Science and Engineering》 2011-04
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Particle Size Control and Luminescence Properties of SrAl_2O_4∶Eu~(2+),Dy~(3+) Prepared by Low Temperature Self-propagating

ZHOU Guo-yong,SU Yu-jing,HUANG Zhi-qiang,DENG Zhi-yong,CHEN Xing-tian(Department of Chemical and Biological Engineering,Hezhou University,He zhou 542800,China)  
SrAl2O4∶Eu2+,Dy3+ was prepared by low temperature self-propagating synthesis at 600℃.The particle size can be controlled effectively by increasing the amount of PEG.The crystal structure,morphology and optical properties of the composites were characterized with the help of X-ray powder diffractometry(XRD),scanning electron microscopy(SEM),photo luminescent(PL) spectroscopy.The size of the powder was decreased with increasing the amount of PEG.The size of particles is in the range of 0.2~1.2μm when 0.0% PEG was added;the sizes of particles decreased to 0.1~0.8μm when 0.4% PEG was added,to 0.1~0.5μm when 0.6% PEG was added.The brightness of phosphors increased while afterglow decay characteristic did not change significantly when PEG was added.The highest brightness with 19110mcd/m2 was obtained when 0.4% PEG was added.The result of experiment indicated that the particle size of SrAl2O4: Eu2+,Dy3+ and its properties of luminescence were effectively controlled by the amount of PEG.Both the PL spectra and luminance decay revealed that this phosphor had efficient luminescence and long-lasting properties and highest intensity emission peak at 516 nm and highest intensity excitation peak at 363nm.An excellent persistent luminescent material was synthesized by low temperature self-propagating.Both the PL spectra and luminance decay revealed that this phosphor had efficient luminescence and long-lasting properties.
【Fund】: 广西壮族自治区教育厅科研资助项目(200911LX443);; 广西高校重点研究实验机构——桂东特色资源开发与利用研究实验室研究资助项目(2009SYS[2]11);; 贺州学院科研资助项目(2009KYYB02)
【CateGory Index】: TQ174.758.23
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