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Preparation and application of graft copolymerization of styrene and acrylate in starch surface sizing agent

WANG Chun-yan, LI Xiao-rui, FEI Gui-qiang, LIU Qin (Key Laboratory of Additives Chemistry & Technology for Light Chemical Industry, Ministry of Education; College of Chemistry and Chemical Engineering, Shaanxi University of Science & Technology, Xi'an 710021, China)  
The starch grafted surface sizing agent was synthesized through free radical polymerization, by using styrene(St), butyl acrylate(BA) and Nhydroxymethyl acrylamide(HMAM) as graft monomers. The effects of the dosage of ammonium persulfate, initiator and monomer on surface siz-ing were studied. The optimum synthesis conditions are as follows: the dosage of ammonium persulfate being 5%, m(FeSO4)/m(H2O2) being 0.03, m(monomer)/ m(strach)=2, m(St)/m(BA)=2, and HMAM dosage being 3%. The sizing degree is more than 60 seconds when the sizing content is 0.09% and the dosage of aluminum sulphate is 0.3%.
【Fund】: 国家自然科学基金项目(20876093 50673055);; 陕西省自然科学基金项目(2007E118)
【CateGory Index】: TS727.5
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