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《Rare Metal Materials and Engineering》 2005-02
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Synthesis and Characterization of TiO_2 Nanotube

Liang Jian, Ma Shufang, Han Peide, Sun Caiyun, Xu Bingshe (Taiyuan University of Technology, Taiyuan 030024, China)  
TiO2 nanotube was synthesized successfully by hydrothermal process, using TiO2 powder and NaOH as the precurser. The micro-morphology and optical properties were characterized by XRD, SEM, HRTEM, UV Absorption Spectra Analyzer and Spectroradiometer, and the formation mechanism was also studied. The results showed that the product is anatase TiO2 nanotube with multiple layers wall, 10 nm~50 nm in the out-diameter, several micron to tens in the length, and opened in both of ends. The formation mechanism of the tube is coordinate with 3-2-1D model. The UV Absorption Spectra and PL spectra showed that the TiO2 nanotubes present blue-shift phenomenon compared to the raw material. The PL spectra also showed that at the visible band the luminous intensity of the TiO2 nanotubes increased obviously.
【Fund】: 国家自然科学基金项目(20271037);; 国家杰出青年科学基金项目(50025103); 国家自然科学基金重大研究计划项目(90306014);; 中日国际合作项目(50311140138)
【CateGory Index】: O614.33
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