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《CHINESE JOURNAL OF MATERIAL RESEARCH》 1997-05
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PREPARATION AND PROPERTIES OF NANOMETER-SIZED TiO_2

WANG Guozhong; WANG Chunchang; MOU Jimei;ZHANG Lide (University of Science and Technology of China)(Institute of Solid State Physics, CAS)  
Using TiCl4 and H2SO4 as reactants, nano-sized TiO2 powder with different grain sizes and an anatase structure was obtained through hydrothermal precipitation method by controlling the conditions of the reaction. Through DSC measurements exothermic peaks were observed in different grain size samples (10nm, 18nm, 29nm), but for 10nm-sample, there is one endothermic peak also. Results of dielectric measurements are as follows: anomalously frequency dependent and grain size effect of dielectric constantwere observed in anatase nano-TiO2 bulk samples. There is one peak in spectra of both dielectric constant and tanδvs temperature.
【Fund】: 国家攀登计划!85-06-03
【CateGory Index】: TB383
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